3-tert-butyloxycarbonylamino-2-methyl-4-(3-nitrophenyl)-6-phenylpyridine

Base Information

Chemical Name:3-tert-butyloxycarbonylamino-2-methyl-4-(3-nitrophenyl)-6-phenylpyridine
CAS No.:127978-25-0
Molecular Formula:C₂₃H₂₃N₃O₄
Molecular Weight:405.453
Hs Code.:

Synonyms:3-tert-butyloxycarbonylamino-2-methyl-4-(3-nitrophenyl)-6-phenylpyridine

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Chemical Property of 3-tert-butyloxycarbonylamino-2-methyl-4-(3-nitrophenyl)-6-phenylpyridine

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Technology Process of 3-tert-butyloxycarbonylamino-2-methyl-4-(3-nitrophenyl)-6-phenylpyridine

There total 1 articles about 3-tert-butyloxycarbonylamino-2-methyl-4-(3-nitrophenyl)-6-phenylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.3%

: 113293-86-0
2-methyl-4-(3-nitrophenyl)-6-phenyl-3-pyridinecarboxylic acid

: 75-65-0
tert-butyl alcohol

: 127978-25-0
3-tert-butyloxycarbonylamino-2-methyl-4-(3-nitrophenyl)-6-phenylpyridine

Guidance literature:: With diphenylphosphoranyl azide; triethylamine; for 14h; Heating;
DOI:10.1248/cpb.41.163

Reference yield: 71.5%

: 127978-25-0
3-tert-butyloxycarbonylamino-2-methyl-4-(3-nitrophenyl)-6-phenylpyridine

: 127978-29-4
3-amino-2-methyl-4-(3-nitrophenyl)-6-phenylpyridine

Guidance literature:: With hydrogenchloride; In ethanol; for 1.5h; Heating;
DOI:10.1248/cpb.41.163

Reference yield:

: 127978-25-0
3-tert-butyloxycarbonylamino-2-methyl-4-(3-nitrophenyl)-6-phenylpyridine

: 127978-36-3
3-(2-bromopropionylamino)-2-methyl-4-(3-nitrophenyl)-6-phenylpyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 71.5 percent / conc. HCl aq. / ethanol / 1.5 h / Heating

2: 68.8 percent / pyridine / toluene / 7 h / Ambient temperature

With pyridine; hydrogenchloride; In ethanol; toluene;
DOI:10.1248/cpb.41.163