[bis(diphenylphosphino)ferrocene]nickel(II)(cyclooctenyl)trifluoroacetate

Base Information

Chemical Name:[bis(diphenylphosphino)ferrocene]nickel(II)(cyclooctenyl)trifluoroacetate
CAS No.:420793-44-8
Molecular Formula:C₂F₃O₂*C₄₂H₄₁FeNiP₂
Molecular Weight:835.288
Hs Code.:

Synonyms:[bis(diphenylphosphino)ferrocene]nickel(II)(cyclooctenyl)trifluoroacetate

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Chemical Property of [bis(diphenylphosphino)ferrocene]nickel(II)(cyclooctenyl)trifluoroacetate

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Technology Process of [bis(diphenylphosphino)ferrocene]nickel(II)(cyclooctenyl)trifluoroacetate

There total 1 articles about [bis(diphenylphosphino)ferrocene]nickel(II)(cyclooctenyl)trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 12150-46-8
1,1'-bis-(diphenylphosphino)ferrocene

: 1295-35-8
bis(1,5-cyclooctadiene)nickel ⁽⁰⁾

: 76-05-1
trifluoroacetic acid

: 420793-44-8
[bis(diphenylphosphino)ferrocene]nickel(II)(cyclooctenyl)trifluoroacetate

Guidance literature:: In benzene; mixt. of Fe-complex, Ni-complex and benzene was stirred for 1 h under N2, TFA was added, stirred at room temp. for 1 h; benzene was evapd. in vacuo, dissolved in THF, filtered, layered with pentane, placed in freezer at -30°C, filtered, washed with pentane,dried in vacuo;
DOI:10.1021/ja017575w

Reference yield: 75.0%

: 420793-44-8
[bis(diphenylphosphino)ferrocene]nickel(II)(cyclooctenyl)trifluoroacetate

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 76-05-1
trifluoroacetic acid

: 420793-79-9
[bis(diphenylphosphino)ferrocene]nickel(II)(cyclopentenyl) trifluoroacetate

Guidance literature:: In tetrahydrofuran; NiFe-complex, 1,3-cyclopentadiene and THF under N2 were stirred for 45 min, TFA was added, stirred at 50°C for 30 min; THF was evapd. in vacuo, dissolved in THF, layered with pentane, placed in freezer at -30°C overnight, filtered, washed with pentane, dried in vacuo;
DOI:10.1021/ja017575w