methyl 2-{[({[4-(methyloxy)phenyl]methyl}amino)carbonyl][(phenylmethyl)oxy]amino}-3-pyridine carboxylate

Base Information

• Chemical Name: methyl 2-{[({[4-(methyloxy)phenyl]methyl}amino)carbonyl][(phenylmethyl)oxy]amino}-3-pyridine carboxylate
• CAS No.: 1312356-05-0
• Molecular Formula: C₂₃H₂₃N₃O₅
• Molecular Weight: 421.453

Synonyms:methyl 2-{[({[4-(methyloxy)phenyl]methyl}amino)carbonyl][(phenylmethyl)oxy]amino}-3-pyridine carboxylate

Chemical Property of methyl 2-{[({[4-(methyloxy)phenyl]methyl}amino)carbonyl][(phenylmethyl)oxy]amino}-3-pyridine carboxylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methyl 2-{[({[4-(methyloxy)phenyl]methyl}amino)carbonyl][(phenylmethyl)oxy]amino}-3-pyridine carboxylate

There total 2 articles about methyl 2-{[({[4-(methyloxy)phenyl]methyl}amino)carbonyl][(phenylmethyl)oxy]amino}-3-pyridine carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

methyl 2-{[(phenylmethyl)oxy]amino}-3-pyridine carboxylate (1312356-04-9) + 4-methoxybenzyl isocyanate (56651-60-6) → methyl 2-{[({[4-(methyloxy)phenyl]methyl}amino)carbonyl][(phenylmethyl)oxy]amino}-3-pyridine carboxylate (1312356-05-0)

Guidance literature:

In 1,2-dichloro-ethane; at 120 ℃; for 1.5h; Microwave irradiation;

DOI:10.1016/j.ejmech.2014.06.061

Reference yield:

2-{[(phenylmethyl)oxy]amino}-3-pyridinecarboxylic acid (1312356-01-6) → methyl 2-{[({[4-(methyloxy)phenyl]methyl}amino)carbonyl][(phenylmethyl)oxy]amino}-3-pyridine carboxylate (1312356-05-0)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid / diethyl ether; methanol; hexane / 0.08 h

2: 1,2-dichloro-ethane / 1.5 h / 120 °C / Microwave irradiation

With acetic acid; In methanol; diethyl ether; hexane; 1,2-dichloro-ethane;

DOI:10.1016/j.ejmech.2014.06.061

Reference yield: 74.0%

methyl 2-{[({[4-(methyloxy)phenyl]methyl}amino)carbonyl][(phenylmethyl)oxy]amino}-3-pyridine carboxylate (1312356-05-0) → C22H19N3O4 (1312356-06-1)

Guidance literature:

With sodium methylate; In methanol; for 0.0833333h;

DOI:10.1016/j.ejmech.2014.06.061

upstream raw materials:

2-{[(phenylmethyl)oxy]amino}-3-pyridinecarboxylic acid

methyl 2-{[(phenylmethyl)oxy]amino}-3-pyridine carboxylate

4-methoxybenzyl isocyanate

Downstream raw materials:

C₂₆H₂₇N₅O₃

1-[(phenylmethyl)oxy]pyrido[2,3-d]pyrimidine-2,4(1H,3H)-dione

4-chloro-1-[(phenylmethyl)oxy]pyrido[2,3-d]pyrimidin-2(1H)-one

1-(benzyloxy)-4-((4-fluorobenzyl)amino)pyrido[2,3-d]pyrimidin-2(1H)-one

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1312356-05-0 methyl 2-{[({[4-(methyloxy)phenyl]methyl}amino)carbonyl][(phenylmethyl)oxy]amino}-3-pyridine carboxylate

Send

Send

Metric Ton KG G Pound L ML

Send

Send