2-methyl-N-((3-methylfuran-2-yl)(p-tolyl)methyl)-N-(prop-2-ynyl)propane-2-sulfonamide

Base Information

Chemical Name:2-methyl-N-((3-methylfuran-2-yl)(p-tolyl)methyl)-N-(prop-2-ynyl)propane-2-sulfonamide
CAS No.:1403651-05-7
Molecular Formula:C₂₀H₂₅NO₃S
Molecular Weight:359.489
Hs Code.:

Synonyms:2-methyl-N-((3-methylfuran-2-yl)(p-tolyl)methyl)-N-(prop-2-ynyl)propane-2-sulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-methyl-N-((3-methylfuran-2-yl)(p-tolyl)methyl)-N-(prop-2-ynyl)propane-2-sulfonamide

Chemical Property:

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Technology Process of 2-methyl-N-((3-methylfuran-2-yl)(p-tolyl)methyl)-N-(prop-2-ynyl)propane-2-sulfonamide

There total 5 articles about 2-methyl-N-((3-methylfuran-2-yl)(p-tolyl)methyl)-N-(prop-2-ynyl)propane-2-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1403651-41-1
2-methyl-N-((3-methylfuran-2-yl)(p-tolyl)methyl)propane-2-sulfonamide

: 106-96-7
propargyl bromide

: 1403651-05-7
2-methyl-N-((3-methylfuran-2-yl)(p-tolyl)methyl)-N-(prop-2-ynyl)propane-2-sulfonamide

Guidance literature:: With caesium carbonate; In acetone; toluene; at 20 ℃;
DOI:10.1002/chem.201200306

Reference yield:

: 20416-16-4
(3-methylfuran-2-yl)methanol

: 1403651-05-7
2-methyl-N-((3-methylfuran-2-yl)(p-tolyl)methyl)-N-(prop-2-ynyl)propane-2-sulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1: manganese(IV) oxide / dichloromethane / 48 h / Reflux

2: triethylamine; titanium tetrachloride / dichloromethane / 0 - 20 °C / Inert atmosphere

3: dichloromethane; tetrahydrofuran / -50 - 20 °C / Inert atmosphere

4: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C

5: caesium carbonate / acetone; toluene / 20 °C

With manganese(IV) oxide; titanium tetrachloride; caesium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; acetone; toluene;
DOI:10.1002/chem.201200306

Reference yield:

: 33342-48-2
3-methyl-2-furfuraldehyde

: 1403651-05-7
2-methyl-N-((3-methylfuran-2-yl)(p-tolyl)methyl)-N-(prop-2-ynyl)propane-2-sulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine; titanium tetrachloride / dichloromethane / 0 - 20 °C / Inert atmosphere

2: dichloromethane; tetrahydrofuran / -50 - 20 °C / Inert atmosphere

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C

4: caesium carbonate / acetone; toluene / 20 °C

With titanium tetrachloride; caesium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; acetone; toluene;
DOI:10.1002/chem.201200306