(S)-methyl 2-((R)-3-(benzylthio)-2-((tert-butoxycarbonyl)amino)propanamido)propanoate

Base Information

Chemical Name:(S)-methyl 2-((R)-3-(benzylthio)-2-((tert-butoxycarbonyl)amino)propanamido)propanoate
CAS No.:57281-70-6
Molecular Formula:C₁₉H₂₈N₂O₅S
Molecular Weight:396.508
Hs Code.:

Synonyms:(S)-methyl 2-((R)-3-(benzylthio)-2-((tert-butoxycarbonyl)amino)propanamido)propanoate

Suppliers and Price of (S)-methyl 2-((R)-3-(benzylthio)-2-((tert-butoxycarbonyl)amino)propanamido)propanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-methyl 2-((R)-3-(benzylthio)-2-((tert-butoxycarbonyl)amino)propanamido)propanoate

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Technology Process of (S)-methyl 2-((R)-3-(benzylthio)-2-((tert-butoxycarbonyl)amino)propanamido)propanoate

There total 2 articles about (S)-methyl 2-((R)-3-(benzylthio)-2-((tert-butoxycarbonyl)amino)propanamido)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 5068-28-0
(2R)-3-benzylsulfanyl-2-tert-butoxycarbonylamino-propionic acid

: 93644-94-1
(S)-methyl 2-(1H-imidazole-1-carboxamido)propanoate

: 57281-70-6
(S)-methyl 2-((R)-3-(benzylthio)-2-((tert-butoxycarbonyl)amino)propanamido)propanoate

Guidance literature:: With benzotriazol-1-ol; copper(ll) bromide; In dichloromethane; at 22 ℃; for 20h; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.201402147

Reference yield:

: 5068-28-0
(2R)-3-benzylsulfanyl-2-tert-butoxycarbonylamino-propionic acid

: 2491-20-5
L-alanine methyl ester hydrochloride

: 57281-70-6
(S)-methyl 2-((R)-3-(benzylthio)-2-((tert-butoxycarbonyl)amino)propanamido)propanoate

: 1610768-82-5
(S)-methyl 2-((S)-3-(benzylthio)-2-((tert-butoxycarbonyl)amino)propanamido)propanoate

Guidance literature:: (2R)-3-benzylsulfanyl-2-tert-butoxycarbonylamino-propionic acid; With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 0.0833333h;

L-alanine methyl ester hydrochloride; In dichloromethane; at 20 ℃; for 2h; Reagent/catalyst; Overall yield = 87 %;
DOI:10.1002/anie.201402147