methyl 4-[4-[(4-chlorophenylsulfonylamino)cycloheptylmethyl]phenyl]butyrate

Base Information

Chemical Name:methyl 4-[4-[(4-chlorophenylsulfonylamino)cycloheptylmethyl]phenyl]butyrate
CAS No.:162938-69-4
Molecular Formula:C₂₅H₃₂ClNO₄S
Molecular Weight:478.052
Hs Code.:

Synonyms:methyl 4-[4-[(4-chlorophenylsulfonylamino)cycloheptylmethyl]phenyl]butyrate

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Chemical Property of methyl 4-[4-[(4-chlorophenylsulfonylamino)cycloheptylmethyl]phenyl]butyrate

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Technology Process of methyl 4-[4-[(4-chlorophenylsulfonylamino)cycloheptylmethyl]phenyl]butyrate

There total 6 articles about methyl 4-[4-[(4-chlorophenylsulfonylamino)cycloheptylmethyl]phenyl]butyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 98-60-2
4-chlorobenzenesulfonyl chloride

: 162941-77-7
4-[4-(Amino-cycloheptyl-methyl)-phenyl]-butyric acid methyl ester

: 162938-69-4
methyl 4-[4-[(4-chlorophenylsulfonylamino)cycloheptylmethyl]phenyl]butyrate

Guidance literature:: With triethylamine; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1248/cpb.45.849

Reference yield:

: 4-(4-Cycloheptanecarbonyl-phenyl)-butyric acid methyl ester

: 162938-69-4
methyl 4-[4-[(4-chlorophenylsulfonylamino)cycloheptylmethyl]phenyl]butyrate

Guidance literature:: Multi-step reaction with 5 steps

1: NaBH₄ / methanol / 1 h / Ambient temperature

2: SOCl₂ / CH₂Cl₂ / 2 h / 40 °C

3: NaN₃ / dimethylformamide / 4.5 h / 80 °C

4: 87 percent / H₂ / PtO₂ / methanol / 5 h / 760 Torr / Ambient temperature

5: 75 percent / Et₃N / CH₂Cl₂ / 2 h / Ambient temperature

With sodium tetrahydroborate; thionyl chloride; sodium azide; hydrogen; triethylamine; platinum(IV) oxide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1248/cpb.45.849

Reference yield:

: 162940-70-7
4-[4-(Cycloheptyl-hydroxy-methyl)-phenyl]-butyric acid methyl ester

: 162938-69-4
methyl 4-[4-[(4-chlorophenylsulfonylamino)cycloheptylmethyl]phenyl]butyrate

Guidance literature:: Multi-step reaction with 4 steps

1: SOCl₂ / CH₂Cl₂ / 2 h / 40 °C

2: NaN₃ / dimethylformamide / 4.5 h / 80 °C

3: 87 percent / H₂ / PtO₂ / methanol / 5 h / 760 Torr / Ambient temperature

4: 75 percent / Et₃N / CH₂Cl₂ / 2 h / Ambient temperature

With thionyl chloride; sodium azide; hydrogen; triethylamine; platinum(IV) oxide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1248/cpb.45.849