p-methoxybenzyl 3-O-allyloxycarbonyl-2,6-dideoxy-α-L-lyxo-hexopyranoside

Base Information

Chemical Name:p-methoxybenzyl 3-O-allyloxycarbonyl-2,6-dideoxy-α-L-lyxo-hexopyranoside
CAS No.:195865-16-8
Molecular Formula:C₁₈H₂₄O₇
Molecular Weight:352.384
Hs Code.:

Synonyms:p-methoxybenzyl 3-O-allyloxycarbonyl-2,6-dideoxy-α-L-lyxo-hexopyranoside

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Chemical Property of p-methoxybenzyl 3-O-allyloxycarbonyl-2,6-dideoxy-α-L-lyxo-hexopyranoside

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Technology Process of p-methoxybenzyl 3-O-allyloxycarbonyl-2,6-dideoxy-α-L-lyxo-hexopyranoside

There total 4 articles about p-methoxybenzyl 3-O-allyloxycarbonyl-2,6-dideoxy-α-L-lyxo-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 2937-50-0
Allyl chloroformate

: 452071-50-0
p-methoxybenzyl 2,6-dideoxy-α-L-lyxo-hexopyranoside

: 195865-16-8
p-methoxybenzyl 3-O-allyloxycarbonyl-2,6-dideoxy-α-L-lyxo-hexopyranoside

Guidance literature:: p-methoxybenzyl 2,6-dideoxy-α-L-lyxo-hexopyranoside; With di(n-butyl)tin oxide; In toluene; for 12h; Heating;

Allyl chloroformate; With triethylamine; In toluene; at -45 ℃; for 2h;

With oxalic acid; In toluene; acetonitrile; at -78 - 20 ℃;
DOI:10.1016/S0968-0896(01)00411-4

Reference yield:

: 105-13-5
4-Methoxybenzyl alcohol

: 195865-16-8
p-methoxybenzyl 3-O-allyloxycarbonyl-2,6-dideoxy-α-L-lyxo-hexopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: 9 g / Ph₃P*HBr / CH₂Cl₂ / 1 h / 20 °C

2.1: 3.5 g / MeONa / methanol / 2 h / 20 °C

3.1: Bu₂SnO / toluene / 12 h / Heating

3.2: Et₃N / toluene / 2 h / -45 °C

3.3: 62 percent / oxalic acid / toluene; acetonitrile / -78 - 20 °C

With sodium methylate; triphenylphosphine hydrobromide; di(n-butyl)tin oxide; In methanol; dichloromethane; toluene;
DOI:10.1016/S0968-0896(01)00411-4

Reference yield:

: 54621-94-2
3,4-di-O-acetyl-L-fucal

: 195865-16-8
p-methoxybenzyl 3-O-allyloxycarbonyl-2,6-dideoxy-α-L-lyxo-hexopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: 9 g / Ph₃P*HBr / CH₂Cl₂ / 1 h / 20 °C

2.1: 3.5 g / MeONa / methanol / 2 h / 20 °C

3.1: Bu₂SnO / toluene / 12 h / Heating

3.2: Et₃N / toluene / 2 h / -45 °C

3.3: 62 percent / oxalic acid / toluene; acetonitrile / -78 - 20 °C

With sodium methylate; triphenylphosphine hydrobromide; di(n-butyl)tin oxide; In methanol; dichloromethane; toluene;
DOI:10.1016/S0968-0896(01)00411-4