chlorooxoacetic acid isobutyl ester

Base Information

Chemical Name:chlorooxoacetic acid isobutyl ester
CAS No.:86141-30-2
Molecular Formula:C₆H₉ClO₃
Molecular Weight:164.589
Hs Code.:

Synonyms:chlorooxoacetic acid isobutyl ester

Suppliers and Price of chlorooxoacetic acid isobutyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of chlorooxoacetic acid isobutyl ester

Chemical Property:

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Technology Process of chlorooxoacetic acid isobutyl ester

There total 1 articles about chlorooxoacetic acid isobutyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 507-20-0
tertiary butyl chloride

: 86141-30-2
chlorooxoacetic acid isobutyl ester

Guidance literature:: at 200 ℃;

Reference yield:

: 86141-30-2
chlorooxoacetic acid isobutyl ester

: 613-94-5
benzoic acid hydrazide

: C₁₃H₁₆N₂O₄

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 8h;
DOI:10.1021/acs.orglett.6b02768

Reference yield:

: 86141-30-2
chlorooxoacetic acid isobutyl ester

: (2s*,3aR*,3a¹r*,5E,9E,10aS*)-isobutyl 5,9-dibenzylidene-3a,10a-dimethyl-2,3,3a,4,5,9,10,10a-octahydro-1H-2,3a¹-epoxypyrene-2-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane / 8 h / 0 - 20 °C

2: triethylamine; p-toluenesulfonyl chloride

3: silver(I) acetate; 2-phenoxyacetic acid; tris(acetonitrile)(η5-pentamethylcyclopentadienyl)rhodium(III) hexafluoroantimonate / 1,2-dichloro-ethane / 11 h / 100 °C

4: potassium carbonate / 1,3,5-trimethyl-benzene / 10 h / 240 °C

With tris(acetonitrile)(η5-pentamethylcyclopentadienyl)rhodium(III) hexafluoroantimonate; silver(I) acetate; potassium carbonate; triethylamine; p-toluenesulfonyl chloride; 2-phenoxyacetic acid; In dichloromethane; 1,2-dichloro-ethane; 1,3,5-trimethyl-benzene;
DOI:10.1021/acs.orglett.6b02768