5-[3,5-bis-(1,3-dioxo-1,3-dihydro-isobenzofuran-5-yloxy)-phenoxy]-2-(4-nitro-phenyl)-isoindole-1,3-dione

Base Information

Chemical Name:5-[3,5-bis-(1,3-dioxo-1,3-dihydro-isobenzofuran-5-yloxy)-phenoxy]-2-(4-nitro-phenyl)-isoindole-1,3-dione
CAS No.:444717-63-9
Molecular Formula:C₃₆H₁₆N₂O₁₃
Molecular Weight:684.529
Hs Code.:

Synonyms:5-[3,5-bis-(1,3-dioxo-1,3-dihydro-isobenzofuran-5-yloxy)-phenoxy]-2-(4-nitro-phenyl)-isoindole-1,3-dione

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Chemical Property of 5-[3,5-bis-(1,3-dioxo-1,3-dihydro-isobenzofuran-5-yloxy)-phenoxy]-2-(4-nitro-phenyl)-isoindole-1,3-dione

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Technology Process of 5-[3,5-bis-(1,3-dioxo-1,3-dihydro-isobenzofuran-5-yloxy)-phenoxy]-2-(4-nitro-phenyl)-isoindole-1,3-dione

There total 6 articles about 5-[3,5-bis-(1,3-dioxo-1,3-dihydro-isobenzofuran-5-yloxy)-phenoxy]-2-(4-nitro-phenyl)-isoindole-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₆H₂₀N₂O₁₅

: 444717-63-9
5-[3,5-bis-(1,3-dioxo-1,3-dihydro-isobenzofuran-5-yloxy)-phenoxy]-2-(4-nitro-phenyl)-isoindole-1,3-dione

Guidance literature:: With acetic anhydride; In acetic acid; at 120 ℃; for 1h;
DOI:10.1021/ma012113o

Reference yield:

: C₃₆H₂₂N₂O₁₆

: 444717-63-9
5-[3,5-bis-(1,3-dioxo-1,3-dihydro-isobenzofuran-5-yloxy)-phenoxy]-2-(4-nitro-phenyl)-isoindole-1,3-dione

Guidance literature:: C₃₆H₂₂N₂O₁₆; With pyridine; acetic anhydride; acetic acid; at 115 ℃;

With acetic anhydride; acetic acid; at 120 ℃; for 1h;
DOI:10.1021/ma021328a

Reference yield:

: 108-73-6
3,5-dihydroxyphenol

: 444717-63-9
5-[3,5-bis-(1,3-dioxo-1,3-dihydro-isobenzofuran-5-yloxy)-phenoxy]-2-(4-nitro-phenyl)-isoindole-1,3-dione

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / 48 h / 20 °C

2: potassium hydroxide / H₂O / 4 h / 136 °C

3: potassium carbonate / N,N-dimethyl-acetamide

4: acetic anhydride / acetic acid / 1 h / 120 °C

With potassium hydroxide; acetic anhydride; potassium carbonate; In N,N-dimethyl acetamide; water; acetic acid;
DOI:10.1021/ma012113o