3-Pyridinol,2-amino-4,6-dimethyl-(9CI)

Base Information

Chemical Name:3-Pyridinol,2-amino-4,6-dimethyl-(9CI)
CAS No.:213685-57-5
Molecular Formula:C₇H₁₀N₂O
Molecular Weight:138.169
Hs Code.:
Mol file:213685-57-5.mol

Synonyms:3-Pyridinol,2-amino-4,6-dimethyl-(9CI)

Suppliers and Price of 3-Pyridinol,2-amino-4,6-dimethyl-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Biosynth Carbosynth
2-Amino-3-hydroxy-4,6-dimethylpyridine
10 g
$ 3250.00

Biosynth Carbosynth
2-Amino-3-hydroxy-4,6-dimethylpyridine
5 g
$ 2800.00

Biosynth Carbosynth
2-Amino-3-hydroxy-4,6-dimethylpyridine
2 g
$ 2000.00

Biosynth Carbosynth
2-Amino-3-hydroxy-4,6-dimethylpyridine
1 g
$ 1500.00

American Custom Chemicals Corporation
2-AMINO-3-HYDROXY-4,6-DIMETHYLPYRIDINE 95.00%
5MG
$ 499.38

AK Scientific
2-Amino-3-hydroxy-4,6-dimethylpyridine
1g
$ 2075.00

Total 6 raw suppliers

Chemical Property of 3-Pyridinol,2-amino-4,6-dimethyl-(9CI)

Chemical Property:

Boiling Point:335.1±42.0 °C(Predicted)
PKA:5.82±0.28(Predicted)
PSA：59.14000
Density:1.191±0.06 g/cm3(Predicted)
LogP:1.56740

Purity/Quality:

99% ^*data from raw suppliers

2-Amino-3-hydroxy-4,6-dimethylpyridine ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-Pyridinol,2-amino-4,6-dimethyl-(9CI)

There total 5 articles about 3-Pyridinol,2-amino-4,6-dimethyl-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4,6-dimethyl-3-hydroxy-2-nitropyridine

: 213685-57-5
2-amino-3-hydroxy-4,6-dimethylpyridine

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethyl acetate; at 20 ℃; for 16h;
DOI:10.1039/c6ob00244g

Reference yield:

: 108-47-4
2,4-lutidine

: 213685-57-5
2-amino-3-hydroxy-4,6-dimethylpyridine

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuric acid; potassium nitrate / 16 h / 100 - 120 °C / Cooling with ice

2: palladium 10% on activated carbon; hydrogen / methanol / 16 h / 20 °C / 760.05 Torr

3: sulfuric acid; sodium nitrite / water / 0.5 h / 0 °C / Reflux

4: ammonium cerium (IV) nitrate; sodium hydrogencarbonate / acetonitrile / 6 h / 20 °C / Reflux

5: palladium 10% on activated carbon; hydrogen / ethyl acetate / 16 h / 20 °C

With ammonium cerium (IV) nitrate; sulfuric acid; palladium 10% on activated carbon; hydrogen; sodium hydrogencarbonate; potassium nitrate; sodium nitrite; In methanol; water; ethyl acetate; acetonitrile;
DOI:10.1039/c6ob00244g

Reference yield:

: 1074-99-3
2,4-dimethyl-5-nitropyridine

: 213685-57-5
2-amino-3-hydroxy-4,6-dimethylpyridine

Guidance literature:: Multi-step reaction with 4 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 16 h / 20 °C / 760.05 Torr

2: sulfuric acid; sodium nitrite / water / 0.5 h / 0 °C / Reflux

3: ammonium cerium (IV) nitrate; sodium hydrogencarbonate / acetonitrile / 6 h / 20 °C / Reflux

4: palladium 10% on activated carbon; hydrogen / ethyl acetate / 16 h / 20 °C

With ammonium cerium (IV) nitrate; sulfuric acid; palladium 10% on activated carbon; hydrogen; sodium hydrogencarbonate; sodium nitrite; In methanol; water; ethyl acetate; acetonitrile;
DOI:10.1039/c6ob00244g