N(2)-(N,N-dimethylaminomethylene)-3-[2-(4-nitrophenyl)ethyl]-6-[(2,3,4,6-tetra-O-benzoyl-β-D-glycopyranosyloxy)methyl]pterin

Base Information

• Chemical Name: N(2)-(N,N-dimethylaminomethylene)-3-[2-(4-nitrophenyl)ethyl]-6-[(2,3,4,6-tetra-O-benzoyl-β-D-glycopyranosyloxy)methyl]pterin
• CAS No.: 1225517-14-5
• Molecular Formula: C₅₂H₄₅N₇O₁₃
• Molecular Weight: 975.968

Synonyms:N(2)-(N,N-dimethylaminomethylene)-3-[2-(4-nitrophenyl)ethyl]-6-[(2,3,4,6-tetra-O-benzoyl-β-D-glycopyranosyloxy)methyl]pterin

Chemical Property of N(2)-(N,N-dimethylaminomethylene)-3-[2-(4-nitrophenyl)ethyl]-6-[(2,3,4,6-tetra-O-benzoyl-β-D-glycopyranosyloxy)methyl]pterin

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Technology Process of N(2)-(N,N-dimethylaminomethylene)-3-[2-(4-nitrophenyl)ethyl]-6-[(2,3,4,6-tetra-O-benzoyl-β-D-glycopyranosyloxy)methyl]pterin

There total 2 articles about N(2)-(N,N-dimethylaminomethylene)-3-[2-(4-nitrophenyl)ethyl]-6-[(2,3,4,6-tetra-O-benzoyl-β-D-glycopyranosyloxy)methyl]pterin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

2,3,4,6-tetra-O-benzoylglucosyl bromide (14218-11-2) + N(2)-(N,N-dimethylaminomethylene)-6-hydroxymethyl-3-[2-(4-nitrophenyl)ethyl]pterin (1225517-13-4) → N(2)-(N,N-dimethylaminomethylene)-3-[2-(4-nitrophenyl)ethyl]-6-[(2,3,4,6-tetra-O-benzoyl-β-D-glycopyranosyloxy)methyl]pterin (1225517-14-5)

Guidance literature:

With silver trifluoromethanesulfonate; tetramethylurea; In chloroform; at 20 ℃; for 6h; Reflux;

DOI:10.3987/COM-09-S(S)78

Reference yield: 43.0%

2,3,4,6-tetra-O-benzoylglucosyl bromide (14218-11-2) + N(2)-(N,N-dimethylaminomethylene)-6-hydroxymethyl-3-[2-(4-nitrophenyl)ethyl]pterin (1225517-13-4) → 6-benzoyloxy-N(2)-(N,N-dimethylaminomethylene)-3-[2-(4-nitrophenyl)ethyl]pterin (1225517-19-0) + N(2)-(N,N-dimethylaminomethylene)-3-[2-(4-nitrophenyl)ethyl]-6-[(2,3,4,6-tetra-O-benzoyl-β-D-glycopyranosyloxy)methyl]pterin (1225517-14-5)

Guidance literature:

With silver trifluoromethanesulfonate; tetramethylurea; In chloroform; at 20 ℃; for 6h; Reflux;

DOI:10.3987/COM-09-S(S)78

Reference yield:

N(2)-(N,N-dimethylaminomethylene)-3-[2-(4-nitrophenyl)ethyl]-6-[(2,3,4,6-tetra-O-benzoyl-β-D-glycopyranosyloxy)methyl]pterin (1225517-14-5) → C24H29N7O9

Guidance literature:

With sodium methylate; In methanol; dichloromethane; at 0 - 20 ℃;

DOI:10.3987/COM-09-S(S)78

upstream raw materials:

2,3,4,6-tetra-O-benzoylglucosyl bromide

N⁽²⁾-(N,N-dimethylaminomethylene)-6-hydroxymethyl-3-[2-(4-nitrophenyl)ethyl]pterin

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