N⁶-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenosine 2'-(2,5-dichlorophenyl triethylammonium phosphate)

Base Information

• Chemical Name: N⁶-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenosine 2'-(2,5-dichlorophenyl triethylammonium phosphate)
• CAS No.: 132849-83-3
• Molecular Formula: C₆H₁₅N*C₄₉H₅₀Cl₂N₅O₉PSi
• Molecular Weight: 1084.12

Synonyms:N⁶-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenosine 2'-(2,5-dichlorophenyl triethylammonium phosphate)

Chemical Property of N⁶-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenosine 2'-(2,5-dichlorophenyl triethylammonium phosphate)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of N⁶-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenosine 2'-(2,5-dichlorophenyl triethylammonium phosphate)

There total 4 articles about N⁶-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenosine 2'-(2,5-dichlorophenyl triethylammonium phosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

N6-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenosine 2'-(2,5-dichlorophenyl 2-cyanoethyl phosphate) (132849-81-1) + triethylamine (121-44-8) → N6-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenosine 2'-(2,5-dichlorophenyl triethylammonium phosphate) (132849-83-3)

Guidance literature:

With water; In pyridine; for 1.5h; Ambient temperature;

DOI:10.1002/hlca.19910740104

Reference yield:

2,5-dichlorophenyl phosphorodichloridate (53676-18-9) → N6-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenosine 2'-(2,5-dichlorophenyl triethylammonium phosphate) (132849-83-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 1,2,4-triazole, pyridine / 30 h / 0 °C

2: 1,2,4-triazole, pyridine / 12 h / Ambient temperature

3: 87 percent / H₂O / pyridine / 1.5 h / Ambient temperature

With pyridine; 1,2,4-Triazole; water; In pyridine;

DOI:10.1002/hlca.19910740104

Reference yield:

N6-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenosine (69504-10-5) → N6-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenosine 2'-(2,5-dichlorophenyl triethylammonium phosphate) (132849-83-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 1,2,4-triazole, pyridine / 30 h / 0 °C

2: 1,2,4-triazole, pyridine / 12 h / Ambient temperature

3: 87 percent / H₂O / pyridine / 1.5 h / Ambient temperature

With pyridine; 1,2,4-Triazole; water; In pyridine;

DOI:10.1002/hlca.19910740104

upstream raw materials:

N⁶-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenosine 2'-(2,5-dichlorophenyl 2-cyanoethyl phosphate)

triethylamine

2,5-dichlorophenyl phosphorodichloridate

N⁶-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenosine

Downstream raw materials:

N⁶-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenylyl-<2'-P-(2,5-dichlorophenyl)>->5'>-N⁶-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>adenosine 2'-(2,5-dichlorophenyl 2-cyanoethyl phosphate)

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