(2,4-dibenzyloxy-6-methoxy)-tolyl-3-(7-hydroxy-6-methyl-5-methoxy)-flavanonyl-8-phenylmethane

Base Information

Chemical Name:(2,4-dibenzyloxy-6-methoxy)-tolyl-3-(7-hydroxy-6-methyl-5-methoxy)-flavanonyl-8-phenylmethane
CAS No.:74627-87-5
Molecular Formula:C₄₆H₄₂O₇
Molecular Weight:706.835
Hs Code.:

Synonyms:(2,4-dibenzyloxy-6-methoxy)-tolyl-3-(7-hydroxy-6-methyl-5-methoxy)-flavanonyl-8-phenylmethane

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Chemical Property of (2,4-dibenzyloxy-6-methoxy)-tolyl-3-(7-hydroxy-6-methyl-5-methoxy)-flavanonyl-8-phenylmethane

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Technology Process of (2,4-dibenzyloxy-6-methoxy)-tolyl-3-(7-hydroxy-6-methyl-5-methoxy)-flavanonyl-8-phenylmethane

There total 12 articles about (2,4-dibenzyloxy-6-methoxy)-tolyl-3-(7-hydroxy-6-methyl-5-methoxy)-flavanonyl-8-phenylmethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1230-20-2
(+/-)-7-Hydroxy-5-methoxy-6-methyl-flavanone

: 74627-96-6
2,6-dibenzyloxy-3-methyl-4-methoxy-diphenylcarbinol

: 74627-87-5
(2,4-dibenzyloxy-6-methoxy)-tolyl-3-(7-hydroxy-6-methyl-5-methoxy)-flavanonyl-8-phenylmethane

Guidance literature:: With boron trifluoride diethyl etherate; In 1,4-dioxane; for 0.5h; Ambient temperature;
DOI:10.1016/0040-4020(82)85056-4

Reference yield:

: 68223-56-3
3-methyl-2,4,6-trihydroxybenzophenone

: 74627-87-5
(2,4-dibenzyloxy-6-methoxy)-tolyl-3-(7-hydroxy-6-methyl-5-methoxy)-flavanonyl-8-phenylmethane

Guidance literature:: Multi-step reaction with 7 steps

1: 55 percent / K₂CO₃ / acetone / 1 h

2: 97 percent / K₂CO₃ / dimethylformamide / 0.42 h / Heating

3: 89 percent / 10percent HCl / methanol / 0.67 h / Heating

4: 96 percent / K₂CO₃ / acetone / 0.17 h / Heating

5: 51 percent / K₂CO₃ / dimethylformamide / 0.33 h / Heating

6: 93 percent / LiAlH₄ / diethyl ether / 1 h / Ambient temperature

7: 83 percent / BF₃-etherate / dioxane / 0.5 h / Ambient temperature

With hydrogenchloride; lithium aluminium tetrahydride; boron trifluoride diethyl etherate; potassium carbonate; In 1,4-dioxane; methanol; diethyl ether; N,N-dimethyl-formamide; acetone;
DOI:10.1016/0040-4020(82)85056-4

Reference yield:

: 74627-92-2
2-benzyloxy-3-methyl-4,6-dihydroxy-benzophenone

: 74627-87-5
(2,4-dibenzyloxy-6-methoxy)-tolyl-3-(7-hydroxy-6-methyl-5-methoxy)-flavanonyl-8-phenylmethane

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / K₂CO₃ / acetone / 0.17 h / Heating

2: 51 percent / K₂CO₃ / dimethylformamide / 0.33 h / Heating

3: 93 percent / LiAlH₄ / diethyl ether / 1 h / Ambient temperature

4: 83 percent / BF₃-etherate / dioxane / 0.5 h / Ambient temperature

With lithium aluminium tetrahydride; boron trifluoride diethyl etherate; potassium carbonate; In 1,4-dioxane; diethyl ether; N,N-dimethyl-formamide; acetone;
DOI:10.1016/0040-4020(82)85056-4