N-benzyloxy acrylamide

Base Information

• Chemical Name: N-benzyloxy acrylamide
• CAS No.: 157614-53-4
• Molecular Formula: C₁₀H₁₁NO₂
• Molecular Weight: 177.203
• Mol file: 157614-53-4.mol

Synonyms:N-benzyloxy acrylamide

Chemical Property of N-benzyloxy acrylamide

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of N-benzyloxy acrylamide

There total 1 articles about N-benzyloxy acrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

N-benzyloxyamine (622-33-3) + acryloyl chloride (814-68-6,25189-84-8) → N-benzyloxy acrylamide (157614-53-4)

Guidance literature:

With triethylamine; In benzene; at 0 - 20 ℃; for 16h;

DOI:10.1016/S0040-4039(00)77052-3

Reference yield: 85.0%

1-dodecene (112-41-4,25067-08-7,62132-67-6) + N-benzyloxy acrylamide (157614-53-4) → (E)-N-(benzyloxy)tridec-2-enamide

Guidance literature:

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; for 6h; Reflux; Inert atmosphere;

DOI:10.3762/bjoc.14.285

Reference yield: 81.0%

1-Decene (872-05-9,17438-89-0,25189-70-2) + N-benzyloxy acrylamide (157614-53-4) → (E)-N-(benzyloxy)undec-2-enamide

Guidance literature:

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; for 6h; Reflux; Inert atmosphere;

DOI:10.3762/bjoc.14.285

upstream raw materials:

N-benzyloxyamine

acryloyl chloride

Downstream raw materials:

N-Benzyloxy-3-piperidin-1-yl-propionamide

N-Benzyloxy-3-[4-(2-benzyloxycarbamoyl-ethyl)-piperazin-1-yl]-propionamide

N-Benzyloxy-3-({6-[(2-benzyloxycarbamoyl-ethyl)-methyl-amino]-hexyl}-methyl-amino)-propionamide

N-Benzyloxy-3-((2-benzyloxycarbamoyl-ethyl)-{3-[(2-benzyloxycarbamoyl-ethyl)-methyl-amino]-propyl}-amino)-propionamide