1,3-Dimethyl-9-<(4-methoxyphenyl)methyl>-6-hydroxypyrimido<2,1-f>purine-2,4,8(1H,3H,9H)-trione

Base Information

Chemical Name:1,3-Dimethyl-9-<(4-methoxyphenyl)methyl>-6-hydroxypyrimido<2,1-f>purine-2,4,8(1H,3H,9H)-trione
CAS No.:120144-42-5
Molecular Formula:C₁₈H₁₇N₅O₅
Molecular Weight:383.363
Hs Code.:

Synonyms:1,3-Dimethyl-9-<(4-methoxyphenyl)methyl>-6-hydroxypyrimido<2,1-f>purine-2,4,8(1H,3H,9H)-trione

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Chemical Property of 1,3-Dimethyl-9-<(4-methoxyphenyl)methyl>-6-hydroxypyrimido<2,1-f>purine-2,4,8(1H,3H,9H)-trione

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Technology Process of 1,3-Dimethyl-9-<(4-methoxyphenyl)methyl>-6-hydroxypyrimido<2,1-f>purine-2,4,8(1H,3H,9H)-trione

There total 1 articles about 1,3-Dimethyl-9-<(4-methoxyphenyl)methyl>-6-hydroxypyrimido<2,1-f>purine-2,4,8(1H,3H,9H)-trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 102212-34-0
8-<<(4-Methoxyphenyl)methyl>amino>theophylline

: 105-53-3
diethyl malonate

: 120144-42-5
1,3-Dimethyl-9-<(4-methoxyphenyl)methyl>-6-hydroxypyrimido<2,1-f>purine-2,4,8(1H,3H,9H)-trione

Guidance literature:: DOI:10.1021/jm00125a029

Reference yield: 28.0%

: 120144-42-5
1,3-Dimethyl-9-<(4-methoxyphenyl)methyl>-6-hydroxypyrimido<2,1-f>purine-2,4,8(1H,3H,9H)-trione

: 120120-91-4
2,3-Dihydro-1,3-dimethyl-9-<(4-methoxyphenyl)methyl>-6-hydroxypyrimido<2,1-f>purine-4,8(1H,9H)-dione

Guidance literature:: With lithium borohydride; In 1,4-dioxane; Heating;
DOI:10.1021/jm00125a029

Reference yield:

: 120144-42-5
1,3-Dimethyl-9-<(4-methoxyphenyl)methyl>-6-hydroxypyrimido<2,1-f>purine-2,4,8(1H,3H,9H)-trione

: 2,3-dihydro-1,3-dimethyl-9-(4-methoxybenzyl)-6-hydroxy-7-(3-methyl-2-butenyl)-pyrimido[2,1-f]purine-4,8(1H,9H)-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 28 percent / LiBH₄ / dioxane / Heating

2: 27 percent

With lithium borohydride; In 1,4-dioxane;
DOI:10.1021/jm00125a029