N-[2-[(2,5-dichloropyrimidin-4-yl)amino]-5-methoxyphenyl]methanesulfonamide

Base Information

Chemical Name:N-[2-[(2,5-dichloropyrimidin-4-yl)amino]-5-methoxyphenyl]methanesulfonamide
CAS No.:1187344-41-7
Molecular Formula:C₁₂H₁₂Cl₂N₄O₃S
Molecular Weight:363.224
Hs Code.:

Synonyms:N-[2-[(2,5-dichloropyrimidin-4-yl)amino]-5-methoxyphenyl]methanesulfonamide

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Chemical Property of N-[2-[(2,5-dichloropyrimidin-4-yl)amino]-5-methoxyphenyl]methanesulfonamide

Chemical Property:

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Technology Process of N-[2-[(2,5-dichloropyrimidin-4-yl)amino]-5-methoxyphenyl]methanesulfonamide

There total 5 articles about N-[2-[(2,5-dichloropyrimidin-4-yl)amino]-5-methoxyphenyl]methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1258423-42-5
N₁-(2,5-dichloropyrimidin-4-yl)-4-methoxybenzene-1,2-diamine

: 124-63-0
methanesulfonyl chloride

: 1187344-41-7
N-[2-[(2,5-dichloropyrimidin-4-yl)amino]-5-methoxyphenyl]methanesulfonamide

Guidance literature:: With pyridine; at 0 - 20 ℃; for 4h;

Reference yield:

: 78136-55-7
1-(benzyloxy)-2-methoxy-4-methylbenzene

: 1187344-41-7
N-[2-[(2,5-dichloropyrimidin-4-yl)amino]-5-methoxyphenyl]methanesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid; nitric acid / 3 h / 4 - 6 °C

2: iron; ammonium chloride / methanol; water / 12 h / 65 °C

3: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 1 h / 0 - 20 °C

4: pyridine / 4 h / 0 - 20 °C

With pyridine; nitric acid; iron; ammonium chloride; acetic acid; N-ethyl-N,N-diisopropylamine; In methanol; water; isopropyl alcohol;

Reference yield:

: 121086-26-8
1-benzyloxy-2-methoxy-4-methyl-5-nitrobenzene

: 1187344-41-7
N-[2-[(2,5-dichloropyrimidin-4-yl)amino]-5-methoxyphenyl]methanesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: iron; ammonium chloride / methanol; water / 12 h / 65 °C

2: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 1 h / 0 - 20 °C

3: pyridine / 4 h / 0 - 20 °C

With pyridine; iron; ammonium chloride; N-ethyl-N,N-diisopropylamine; In methanol; water; isopropyl alcohol;