N-(6'-chloro-1,1'-dimethyl-1H,1'H-[3,3'-biindol]-2-yl)-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-(6'-chloro-1,1'-dimethyl-1H,1'H-[3,3'-biindol]-2-yl)-4-methylbenzenesulfonamide
CAS No.:1562571-47-4
Molecular Formula:C₂₅H₂₂ClN₃O₂S
Molecular Weight:463.988
Hs Code.:

Synonyms:N-(6'-chloro-1,1'-dimethyl-1H,1'H-[3,3'-biindol]-2-yl)-4-methylbenzenesulfonamide

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Chemical Property of N-(6'-chloro-1,1'-dimethyl-1H,1'H-[3,3'-biindol]-2-yl)-4-methylbenzenesulfonamide

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Technology Process of N-(6'-chloro-1,1'-dimethyl-1H,1'H-[3,3'-biindol]-2-yl)-4-methylbenzenesulfonamide

There total 4 articles about N-(6'-chloro-1,1'-dimethyl-1H,1'H-[3,3'-biindol]-2-yl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1562569-28-1
4-methyl-3-tosyl-3,4-dihydro-[1,2,3]triazolo[4,5-b]indole

: 155868-51-2
6-chloro-1-methyl-1H-indole

: 1562571-47-4
N-(6'-chloro-1,1'-dimethyl-1H,1'H-[3,3'-biindol]-2-yl)-4-methylbenzenesulfonamide

Guidance literature:: With rhodium (II) octanoate dimer; In toluene; at 80 ℃; regioselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1021/ol5002347

Reference yield: 87.0%

: N-(1-methylindol-2-ylidene-3-diazo)-4-methylbenzene-1-sulfonamide

: 155868-51-2
6-chloro-1-methyl-1H-indole

: 1562571-47-4
N-(6'-chloro-1,1'-dimethyl-1H,1'H-[3,3'-biindol]-2-yl)-4-methylbenzenesulfonamide

Guidance literature:: With copper(II) bis(trifluoromethanesulfonate); In 1,2-dichloro-ethane; at 20 ℃; for 3h; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.5b00089

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 1562571-47-4
N-(6'-chloro-1,1'-dimethyl-1H,1'H-[3,3'-biindol]-2-yl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide / ethanol; water / 3 h / 20 °C / Heating

2: copper(l) chloride; triethylamine / acetonitrile / 3 h / 20 °C / Inert atmosphere; Schlenk technique

3: rhodium (II) octanoate dimer / toluene / 80 °C / Inert atmosphere; Schlenk technique

With sodium azide; rhodium (II) octanoate dimer; triethylamine; copper(l) chloride; In ethanol; water; toluene; acetonitrile;
DOI:10.1021/ol5002347