Technology Process of C37H50O5
There total 5 articles about C37H50O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydride;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 3h;
Inert atmosphere;
DOI:10.1039/c1ob05251a
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: oxygen; palladium dichloride / N,N-dimethyl acetamide / 1 h / 20 °C / 9000.9 Torr
1.2: 12 h / 90 °C / 3000.3 Torr
2.1: lithium iodide / diethyl ether / 0.17 h / -40 °C / Inert atmosphere
2.2: 0.75 h / -100 °C / Inert atmosphere
2.3: -100 - 20 °C
3.1: sodium hydride / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere
With
oxygen; sodium hydride; palladium dichloride; lithium iodide;
In
diethyl ether; N,N-dimethyl acetamide; N,N-dimethyl-formamide;
DOI:10.1039/c1ob05251a
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium iodide / diethyl ether / 0.17 h / -40 °C / Inert atmosphere
1.2: 0.75 h / -100 °C / Inert atmosphere
1.3: -100 - 20 °C
2.1: sodium hydride / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere
With
sodium hydride; lithium iodide;
In
diethyl ether; N,N-dimethyl-formamide;
DOI:10.1039/c1ob05251a