N-Methoxy-N-methyl-2-(phenylsulfinyl)acetamide

Base Information

Chemical Name:N-Methoxy-N-methyl-2-(phenylsulfinyl)acetamide
CAS No.:212180-20-6
Molecular Formula:C₁₀H₁₃NO₃S
Molecular Weight:227.284
Hs Code.:
European Community (EC) Number:664-183-4
DSSTox Substance ID:DTXSID501245909
Nikkaji Number:J979.076D
Mol file:212180-20-6.mol

Synonyms:N-Methoxy-N-methyl-2-(phenylsulfinyl)acetamide;DTXSID501245909;212180-20-6;N-Methyl-N-methoxy-2-(phenylsulfinyl)acetamide

Suppliers and Price of N-Methoxy-N-methyl-2-(phenylsulfinyl)acetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
N-Methoxy-N-methyl-2-(phenylsulfinyl)acetamide Aldrich
1g
$ 55.10

Total 2 raw suppliers

Chemical Property of N-Methoxy-N-methyl-2-(phenylsulfinyl)acetamide

Chemical Property:

Refractive Index:n20/D 1.566(lit.)
Flash Point:110 °C
PSA：65.82000
Density:1.23 g/mL at 25 °C(lit.)
LogP:1.67970
XLogP3:0.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:227.06161445
Heavy Atom Count:15
Complexity:239

Purity/Quality:

99% ^*data from raw suppliers

N-Methoxy-N-methyl-2-(phenylsulfinyl)acetamide Aldrich ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xi
Statements: 36/37/38
Safety Statements: 26-36

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C(=O)CS(=O)C1=CC=CC=C1)OC

Technology Process of N-Methoxy-N-methyl-2-(phenylsulfinyl)acetamide

There total 2 articles about N-Methoxy-N-methyl-2-(phenylsulfinyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 191731-37-0
N-methoxy-N-methyl-2-(phenylthio)acetamide

: 212180-20-6
phenyl(N-methoxy-N-methylcarbamoylmethyl)sulfoxide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 0.25h;
DOI:10.1016/S0040-4039(98)01208-8

Reference yield:

: 930-69-8
sodium thiophenolate

: 212180-20-6
phenyl(N-methoxy-N-methylcarbamoylmethyl)sulfoxide

Guidance literature:: Multi-step reaction with 2 steps

1: 13.4 g / tetrahydrofuran / 12 h / Ambient temperature

2: 7.5 g / mCPBA / CH₂Cl₂ / 0.25 h

With 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(98)01208-8

Reference yield:

: 78-77-3
Isobutyl bromide

: 212180-20-6
phenyl(N-methoxy-N-methylcarbamoylmethyl)sulfoxide

: 170969-86-5
(E)-N-methoxy-N-methyl 4-methyl-pent-2-enamide

Guidance literature:: With sodium hydride; trimethylphosphane; Yield given. Multistep reaction; 1.) DME, 20 min; 2.) DME, 10 min then 120 deg C, 2 h;
DOI:10.1016/S0040-4039(98)01208-8