3-prop-2-enyl-2-prop-2-enylsulfanylspiro[6H-benzo[h]quinazoline-5,1'-cyclohexane]-4-one

Base Information

Chemical Name:3-prop-2-enyl-2-prop-2-enylsulfanylspiro[6H-benzo[h]quinazoline-5,1'-cyclohexane]-4-one
CAS No.:5705-09-9
Molecular Formula:C₁₄H₁₄N₂O₂
Molecular Weight:242.277
Hs Code.:
DSSTox Substance ID:DTXSID20367349
Wikidata:Q82153131

Synonyms:5705-09-9;3-prop-2-enyl-2-prop-2-enylsulfanylspiro[6H-benzo[h]quinazoline-5,1'-cyclohexane]-4-one;3-prop-2-enyl-2-prop-2-enylsulfanylspiro[6H-benzo[h]quinazoline-5,1//'-cyclohexane]-4-one;Oprea1_123110;Oprea1_420378;DTXSID20367349;DARSXULVYWIRGV-UHFFFAOYSA-N;STK833126;AKOS000505270;3-allyl-2-(allylsulfanyl)-5,6-dihydrospiro(benzo[h]quinazoline-5,1'-cyclohexane)-4(3H)-one;AK-968/11841254;3-allyl-2-(allylthio)-3H-spiro[benzo[h]quinazoline-5,1'-cyclohexan]-4(6H)-one;3-(prop-2-en-1-yl)-2-(prop-2-en-1-ylsulfanyl)-3H-spiro[benzo[h]quinazoline-5,1'-cyclohexan]-4(6H)-one

Suppliers and Price of 3-prop-2-enyl-2-prop-2-enylsulfanylspiro[6H-benzo[h]quinazoline-5,1'-cyclohexane]-4-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-prop-2-enyl-2-prop-2-enylsulfanylspiro[6H-benzo[h]quinazoline-5,1'-cyclohexane]-4-one

Chemical Property:

XLogP3:5.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:378.17658463
Heavy Atom Count:27
Complexity:687

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C=CCN1C(=O)C2=C(C3=CC=CC=C3CC24CCCCC4)N=C1SCC=C

Technology Process of 3-prop-2-enyl-2-prop-2-enylsulfanylspiro[6H-benzo[h]quinazoline-5,1'-cyclohexane]-4-one

There total 2 articles about 3-prop-2-enyl-2-prop-2-enylsulfanylspiro[6H-benzo[h]quinazoline-5,1'-cyclohexane]-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 3526-43-0
N-(4-methoxybenzyl)aniline

: 5705-09-9
N-(4-methoxybenzyl)-N-nitrosoaniline

Guidance literature:: With tert.-butylnitrite; In neat (no solvent); at 20 ℃; for 0.25h; chemoselective reaction; Green chemistry;
DOI:10.1039/c5gc02880a

Reference yield:

: 836-41-9
p-methoxybenzylidene-phenylamine

: 5705-09-9
N-(4-methoxybenzyl)-N-nitrosoaniline

Guidance literature:: Multi-step reaction with 2 steps

1: sodium amalgam; alcohol

2: diluted sulfuric acid; sodium nitrite

With sodium amalgam; ethanol; sulfuric acid; sodium nitrite;