3-(3,4-dimethoxyphenyl)phenyl sulfonyl-d/l-Phe(3-acetyl hydroxyamidine)-4-(2-Boc-amidoethyl)piperidide

Base Information

Chemical Name:3-(3,4-dimethoxyphenyl)phenyl sulfonyl-d/l-Phe(3-acetyl hydroxyamidine)-4-(2-Boc-amidoethyl)piperidide
CAS No.:1042927-04-7
Molecular Formula:C₃₈H₄₉N₅O₉S
Molecular Weight:751.901
Hs Code.:

Synonyms:3-(3,4-dimethoxyphenyl)phenyl sulfonyl-d/l-Phe(3-acetyl hydroxyamidine)-4-(2-Boc-amidoethyl)piperidide

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Chemical Property of 3-(3,4-dimethoxyphenyl)phenyl sulfonyl-d/l-Phe(3-acetyl hydroxyamidine)-4-(2-Boc-amidoethyl)piperidide

Chemical Property:

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Technology Process of 3-(3,4-dimethoxyphenyl)phenyl sulfonyl-d/l-Phe(3-acetyl hydroxyamidine)-4-(2-Boc-amidoethyl)piperidide

There total 1 articles about 3-(3,4-dimethoxyphenyl)phenyl sulfonyl-d/l-Phe(3-acetyl hydroxyamidine)-4-(2-Boc-amidoethyl)piperidide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1042927-02-5
3-(3,4-dimethoxyphenyl)phenyl sulfonyl-d/l-Phe(3-CN)-4-(2-Boc-amidoethyl)-piperidide

: 108-24-7
acetic anhydride

: 1042927-04-7
3-(3,4-dimethoxyphenyl)phenyl sulfonyl-d/l-Phe(3-acetyl hydroxyamidine)-4-(2-Boc-amidoethyl)piperidide

Guidance literature:: 3-(3,4-dimethoxyphenyl)phenyl sulfonyl-d/l-Phe(3-CN)-4-(2-Boc-amidoethyl)-piperidide; With hydroxylamine hydrochloride; N-ethyl-N,N-diisopropylamine; In ethanol; at 20 ℃; for 4h;

acetic anhydride; With acetic acid; In ethanol;

Reference yield:

: 1042927-04-7
3-(3,4-dimethoxyphenyl)phenyl sulfonyl-d/l-Phe(3-acetyl hydroxyamidine)-4-(2-Boc-amidoethyl)piperidide

: 76-05-1
trifluoroacetic acid

: 3-(3,4-dimethoxyphenyl)phenyl sulfonyl-d/l-Phe(3-Am)-4-(amino ethyl)piperidide ditrifluoroacetate

Guidance literature:: 3-(3,4-dimethoxyphenyl)phenyl sulfonyl-d/l-Phe(3-acetyl hydroxyamidine)-4-(2-Boc-amidoethyl)piperidide; With hydrogen; palladium 10% on activated carbon; In acetic acid;

trifluoroacetic acid; In acetic acid; for 1h;