Technology Process of C27H31IN2O3
There total 1 articles about C27H31IN2O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C28H30N2O4;
With
Wilkinson's catalyst; benzonitrile;
In
toluene;
at 120 ℃;
phosgene;
With
triethylamine;
In
toluene;
at -45 - 23 ℃;
(Z)-4-bromo-3-iodobut-2-en-1-yl acetate;
Further stages;
DOI:10.1038/nature10232
- Guidance literature:
-
With
tetrabutyl-ammonium chloride; palladium diacetate; sodium hydrogencarbonate;
In
ethyl acetate;
at 23 ℃;
DOI:10.1038/nature10232
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrabutyl-ammonium chloride; palladium diacetate; sodium hydrogencarbonate / ethyl acetate / 23 °C
2: thiophenol; trifluoroacetic acid / 45 °C
3: sodium acetate; acetic anhydride / acetic acid / 120 °C
With
tetrabutyl-ammonium chloride; sodium acetate; palladium diacetate; acetic anhydride; sodium hydrogencarbonate; thiophenol; trifluoroacetic acid;
In
acetic acid; ethyl acetate;
1: Heck reaction;
DOI:10.1038/nature10232