N-benzyl-N-[(S)-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)ethyl]hydroxylamine

Base Information

Chemical Name:N-benzyl-N-[(S)-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)ethyl]hydroxylamine
CAS No.:192764-09-3
Molecular Formula:C₁₄H₂₁NO₃
Molecular Weight:251.326
Hs Code.:

Synonyms:N-benzyl-N-[(S)-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)ethyl]hydroxylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-benzyl-N-[(S)-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)ethyl]hydroxylamine

Chemical Property:

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Technology Process of N-benzyl-N-[(S)-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)ethyl]hydroxylamine

There total 3 articles about N-benzyl-N-[(S)-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)ethyl]hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-16-1
methylmagnesium bromide

: 91190-38-4,111058-38-9,1165677-00-8
N-benzyl-2,3-O-isopropylidene-D-glyceraldehyde nitrone

: 192764-09-3
N-benzyl-N-[(S)-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)ethyl]hydroxylamine

: 192764-08-2
N-benzyl-N-[(R)-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)ethyl]hydroxylamine

Guidance literature:: With diethylaluminium chloride; In diethyl ether; at -40 ℃; for 6h;
DOI:10.1016/S0957-4166(97)00175-4

Reference yield:

: 75-16-1
methylmagnesium bromide

: 91190-38-4,111058-38-9,1165677-00-8
N-benzyl-2,3-O-isopropylidene-D-glyceraldehyde nitrone

: 192764-09-3
N-benzyl-N-[(S)-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)ethyl]hydroxylamine

Guidance literature:: With diethylaluminium chloride; Yield given. Multistep reaction; 1.) Et₂O, room temp., 5 min, 2.) Et₂O, -60 deg C, 6 h;
DOI:10.1021/jo971913n

Reference yield:

: 622-30-0
N-benzyl hydroxylalmine

: 15186-48-8
2,3-isopropylidene-glyceraldehyde

: 192764-09-3
N-benzyl-N-[(S)-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)ethyl]hydroxylamine

: 192764-08-2
N-benzyl-N-[(R)-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)ethyl]hydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium sulfate / dichloromethane / 16.5 h / 20 °C / Inert atmosphere

2.1: diethylaluminium chloride / diethyl ether; hexane / 0.25 h / -60 °C

2.2: 2 h / -60 °C

2.3: 0.25 h / 20 °C

With diethylaluminium chloride; sodium sulfate; In diethyl ether; hexane; dichloromethane;