2,4,6-F₃C₆H₂NSO

Base Information

• Chemical Name: 2,4,6-F₃C₆H₂NSO
• CAS No.: 501670-12-8
• Molecular Formula: C₆H₂F₃NOS
• Molecular Weight: 193.149

Synonyms:2,4,6-F₃C₆H₂NSO

Chemical Property of 2,4,6-F₃C₆H₂NSO

Chemical Property:

Purity/Quality:

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Technology Process of 2,4,6-F₃C₆H₂NSO

There total 1 articles about 2,4,6-F₃C₆H₂NSO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

2,4,6-trifluoroaniline (363-81-5) → 2,4,6-F3C6H2NSO (501670-12-8)

Guidance literature:

With thionyl chloride; In benzene; at 25 ℃; for 10h; Reflux; Inert atmosphere;

DOI:10.1039/c0dt01133a

Reference yield: 95.0%

2,4,6-F3C6H2NSO (501670-12-8) + chromyl chloride (14977-61-8) → [Cr(N-2,4,6-F3C6H2)2Cl2]

Guidance literature:

In tetrachloromethane; byproducts: SO2; Sonication; (Ar) 2 equiv. sulfinyl amine was added to soln. CrO2Cl2 in CCl4, refluxed for 30 min; volatiles were removed in vacuo at 20°C, residue was washed by sonication with pentane and dried in vacuo; elem. anal.;

DOI:10.1039/c0dt01133a

Reference yield: 83.0%

2,4,6-F3C6H2NSO (501670-12-8) + vanadium(V) oxychloride (7727-18-6) + toluene (108-88-3,15644-74-3,16713-13-6) → [V(N-2,4,6-F3C6H2)Cl3]*(toluene)

Guidance literature:

In toluene; byproducts: SO2; Sonication; (Ar) to soln. VOCl3 in toluene soln. ArCSO in toluene was added at room temp., stirred for 1-6 h at room temp.; volatiles were emoved in vacuo at 20°C, residue was suspnd. in pentane by sonication and stored at -80°C for 24 h, ppt. was separated, washed with pre-cooled pentane and dried in vacuo at 20°C; elem. anal.;

DOI:10.1039/c0dt01133a

upstream raw materials:

2,4,6-trifluoroaniline

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