3-<carbamoyl>methyl>-4-methylthiazolium chloride

Base Information

Chemical Name:3-<carbamoyl>methyl>-4-methylthiazolium chloride
CAS No.:123597-16-0
Molecular Formula:C₂₄H₂₇N₄O₃S*Cl
Molecular Weight:487.022
Hs Code.:

3-<<N,N-Bis<(N-benzylcarbamoyl)methyl>carbamoyl>methyl>-4-methylthiazolium chloride

Synonyms:3-<carbamoyl>methyl>-4-methylthiazolium chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-<carbamoyl>methyl>-4-methylthiazolium chloride

Chemical Property:

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Technology Process of 3-<carbamoyl>methyl>-4-methylthiazolium chloride

There total 4 articles about 3-<carbamoyl>methyl>-4-methylthiazolium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123597-18-2
<(Benzyloxy)carbonyl>bis<(N-benzylcarbamoyl)methyl>amine

: 123597-16-0
3-<carbamoyl>methyl>-4-methylthiazolium chloride

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / H₂ / 10percent Pd/C / ethanol / 6 h / 20 °C / 3000.2 Torr

2: 32 percent / Et₃N / CHCl₃ / 1 h / 20 °C

3: 48 h / 20 °C

4: Dowex ion-exchange resin (1X₈, Cl(-)) / H₂O

With Dowex ion-exchange resin (1X₈, Cl(-)); hydrogen; triethylamine; palladium on activated charcoal; In ethanol; chloroform; water;
DOI:10.1021/ja00204a017

Reference yield:

: 3-<carbamoyl>methyl>-4-methylthiazolium bromide

: 123597-16-0
3-<carbamoyl>methyl>-4-methylthiazolium chloride

Guidance literature:: With Dowex ion-exchange resin (1X₈, Cl(-)); In water; Yield given;
DOI:10.1021/ja00204a017

Reference yield:

: 123597-19-3
Bis<(N-benzylcarbamoyl)methyl>amine

: 123597-16-0
3-<carbamoyl>methyl>-4-methylthiazolium chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 32 percent / Et₃N / CHCl₃ / 1 h / 20 °C

2: 48 h / 20 °C

3: Dowex ion-exchange resin (1X₈, Cl(-)) / H₂O

With Dowex ion-exchange resin (1X₈, Cl(-)); triethylamine; In chloroform; water;
DOI:10.1021/ja00204a017