(Z)-3-(4-chloro-2-fluoro-5-nitrophenylamino)-1-(2, 6-dichloropyridin-3-yl)-2-buten-1-one

Base Information

Chemical Name:(Z)-3-(4-chloro-2-fluoro-5-nitrophenylamino)-1-(2, 6-dichloropyridin-3-yl)-2-buten-1-one
CAS No.:1315180-31-4
Molecular Formula:C₁₅H₉Cl₃FN₃O₃
Molecular Weight:404.612
Hs Code.:

Synonyms:(Z)-3-(4-chloro-2-fluoro-5-nitrophenylamino)-1-(2, 6-dichloropyridin-3-yl)-2-buten-1-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-3-(4-chloro-2-fluoro-5-nitrophenylamino)-1-(2, 6-dichloropyridin-3-yl)-2-buten-1-one

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Technology Process of (Z)-3-(4-chloro-2-fluoro-5-nitrophenylamino)-1-(2, 6-dichloropyridin-3-yl)-2-buten-1-one

There total 1 articles about (Z)-3-(4-chloro-2-fluoro-5-nitrophenylamino)-1-(2, 6-dichloropyridin-3-yl)-2-buten-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 86988-02-5
4-chloro-2-fluoro-5-nitroaniline

: 1315179-94-2
(E)-1-(2, 6-dichloropyridin-3-yl)-3-dimethylamino-2-buten-1-one

: 1315180-31-4
(Z)-3-(4-chloro-2-fluoro-5-nitrophenylamino)-1-(2, 6-dichloropyridin-3-yl)-2-buten-1-one

Guidance literature:: With acetic acid; at 60 - 70 ℃; for 5h;

Reference yield:

: 1315180-31-4
(Z)-3-(4-chloro-2-fluoro-5-nitrophenylamino)-1-(2, 6-dichloropyridin-3-yl)-2-buten-1-one

: 1315179-89-5
1-(5-amino-4-chloro-2-fluorophenyl)-7-(3, 5-dimethylisoxazol-4-yl)-2-methyl-1, 4-dihydro-4-oxo-1, 8-naphthyridine

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol; water; ammonium chloride; iron / 0.33 h / Reflux

2: potassium carbonate / dimethyl sulfoxide / 1.5 h / 80 °C

3: triethylamine; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / palladium diacetate / 1,4-dioxane / 2 h / Reflux; Inert atmosphere

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; ethanol; water; iron; potassium carbonate; ammonium chloride; triethylamine; palladium diacetate; In 1,4-dioxane; dimethyl sulfoxide;

Reference yield:

: 1315180-31-4
(Z)-3-(4-chloro-2-fluoro-5-nitrophenylamino)-1-(2, 6-dichloropyridin-3-yl)-2-buten-1-one

: 1315180-33-6
1-(5-amino-4-chloro-2-fluorophenyl)-7-chloro-2-methyl-1, 4-dihydro-4-oxo-1, 8-naphthyridine

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol; water; ammonium chloride; iron / 0.33 h / Reflux

2: potassium carbonate / dimethyl sulfoxide / 1.5 h / 80 °C

With ethanol; water; iron; potassium carbonate; ammonium chloride; In dimethyl sulfoxide;