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Technology Process of C6H2I(OSi(CH3)2C(CH3)3)2CHCOOCH3(NHCOCHNHC6H2Cl2(OSi(CH3)2C(CH3)3)COCHNH(COCOC6H2Cl2OH)(CH2C8H4NH)BO2C6H12)

C6H2I(OSi(CH3)2C(CH3)3)2CHCOOCH3(NHCOCHNHC6H2Cl2(OSi(CH3)2C(CH3)3)COCHNH(COCOC6H2Cl2OH)(CH2C8H4NH)BO2C6H12)

Base Information
  • Chemical Name:C6H2I(OSi(CH3)2C(CH3)3)2CHCOOCH3(NHCOCHNHC6H2Cl2(OSi(CH3)2C(CH3)3)COCHNH(COCOC6H2Cl2OH)(CH2C8H4NH)BO2C6H12)
  • CAS No.:1225383-19-6
  • Molecular Formula:C60H80BCl4IN4O12Si3
  • Molecular Weight:1413.1
  • Hs Code.:
C<sub>6</sub>H<sub>2</sub>I(OSi(CH<sub>3</sub>)2C(CH<sub>3</sub>)3)2CHCOOCH<sub>3</sub>(NHCOCHNHC<sub>6</sub>H<sub>2</sub>Cl<sub>2</sub>(OSi(CH<sub>3</sub>)2C(CH<sub>3</sub>)3)COCHNH(COCOC<sub>6</sub>H<sub>2</sub>Cl<sub>2</sub>OH)(CH<sub>2</sub>C<sub>8</sub>H<sub>4</sub>NH)BO<sub>2</sub>C<sub>6</sub>H<sub>12</sub>)

Synonyms:C6H2I(OSi(CH3)2C(CH3)3)2CHCOOCH3(NHCOCHNHC6H2Cl2(OSi(CH3)2C(CH3)3)COCHNH(COCOC6H2Cl2OH)(CH2C8H4NH)BO2C6H12)

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Chemical Property of C6H2I(OSi(CH3)2C(CH3)3)2CHCOOCH3(NHCOCHNHC6H2Cl2(OSi(CH3)2C(CH3)3)COCHNH(COCOC6H2Cl2OH)(CH2C8H4NH)BO2C6H12)
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Technology Process of C6H2I(OSi(CH3)2C(CH3)3)2CHCOOCH3(NHCOCHNHC6H2Cl2(OSi(CH3)2C(CH3)3)COCHNH(COCOC6H2Cl2OH)(CH2C8H4NH)BO2C6H12)

There total 1 articles about C6H2I(OSi(CH3)2C(CH3)3)2CHCOOCH3(NHCOCHNHC6H2Cl2(OSi(CH3)2C(CH3)3)COCHNH(COCOC6H2Cl2OH)(CH2C8H4NH)BO2C6H12) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2-[2-(3,5-dichloro-4-hydroxy-phenyl)-2-oxo-acetylamino]-3-[6-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-1<i>H</i>-indol-3-yl]-propionic acid
854443-88-2

2-[2-(3,5-dichloro-4-hydroxy-phenyl)-2-oxo-acetylamino]-3-[6-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-1H-indol-3-yl]-propionic acid

C<sub>6</sub>H<sub>2</sub>I(OSi(CH<sub>3</sub>)2(C(CH<sub>3</sub>)3))2CH(COOCH<sub>3</sub>)(NHCOCH(NH<sub>2</sub>)C<sub>6</sub>H<sub>2</sub>Cl<sub>2</sub>(OSi(CH<sub>3</sub>)2(C(CH<sub>3</sub>)3)))

C6H2I(OSi(CH3)2(C(CH3)3))2CH(COOCH3)(NHCOCH(NH2)C6H2Cl2(OSi(CH3)2(C(CH3)3)))

C<sub>6</sub>H<sub>2</sub>I(OSi(CH<sub>3</sub>)2C(CH<sub>3</sub>)3)2CHCOOCH<sub>3</sub>(NHCOCHNHC<sub>6</sub>H<sub>2</sub>Cl<sub>2</sub>(OSi(CH<sub>3</sub>)2C(CH<sub>3</sub>)3)COCHNH(COCOC<sub>6</sub>H<sub>2</sub>Cl<sub>2</sub>OH)(CH<sub>2</sub>C<sub>8</sub>H<sub>4</sub>NH)BO<sub>2</sub>C<sub>6</sub>H<sub>12</sub>)
1225383-19-6

C6H2I(OSi(CH3)2C(CH3)3)2CHCOOCH3(NHCOCHNHC6H2Cl2(OSi(CH3)2C(CH3)3)COCHNH(COCOC6H2Cl2OH)(CH2C8H4NH)BO2C6H12)

Guidance literature:
With 2,5-dimethylpyridine; HATU; In tetrahydrofuran; dichloromethane; at 0 - 25 ℃;
DOI:10.1002/anie.200906797

Reference yield:

C<sub>6</sub>H<sub>2</sub>I(OSi(CH<sub>3</sub>)2C(CH<sub>3</sub>)3)2CHCOOCH<sub>3</sub>(NHCOCHNHC<sub>6</sub>H<sub>2</sub>Cl<sub>2</sub>(OSi(CH<sub>3</sub>)2C(CH<sub>3</sub>)3)COCHNH(COCOC<sub>6</sub>H<sub>2</sub>Cl<sub>2</sub>OH)(CH<sub>2</sub>C<sub>8</sub>H<sub>4</sub>NH)BO<sub>2</sub>C<sub>6</sub>H<sub>12</sub>)
1225383-19-6

C6H2I(OSi(CH3)2C(CH3)3)2CHCOOCH3(NHCOCHNHC6H2Cl2(OSi(CH3)2C(CH3)3)COCHNH(COCOC6H2Cl2OH)(CH2C8H4NH)BO2C6H12)

C<sub>48</sub>H<sub>54</sub>Cl<sub>4</sub>N<sub>4</sub>O<sub>10</sub>Si<sub>2</sub>

C48H54Cl4N4O10Si2

C<sub>54</sub>H<sub>68</sub>Cl<sub>4</sub>N<sub>4</sub>O<sub>10</sub>Si<sub>3</sub>

C54H68Cl4N4O10Si3

Guidance literature:
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; water; potassium carbonate; In 1,4-dioxane; at 90 ℃; Inert atmosphere;
DOI:10.1002/anie.200906797
upstream raw materials:

2-[2-(3,5-dichloro-4-hydroxy-phenyl)-2-oxo-acetylamino]-3-[6-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-1H-indol-3-yl]-propionic acid

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