Ethyl-(10-(<(ethoxycarbonyl)methyl>thio)-7-phenyl-8-thia-6-azaspiro<4.5>deca-6.9-dien-9-carboxylat)

Base Information

Chemical Name:Ethyl-(10-(<(ethoxycarbonyl)methyl>thio)-7-phenyl-8-thia-6-azaspiro<4.5>deca-6.9-dien-9-carboxylat)
CAS No.:158046-97-0
Molecular Formula:C₂₁H₂₅NO₄S₂
Molecular Weight:419.566
Hs Code.:

Synonyms:Ethyl-(10-(<(ethoxycarbonyl)methyl>thio)-7-phenyl-8-thia-6-azaspiro<4.5>deca-6.9-dien-9-carboxylat)

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Chemical Property of Ethyl-(10-(<(ethoxycarbonyl)methyl>thio)-7-phenyl-8-thia-6-azaspiro<4.5>deca-6.9-dien-9-carboxylat)

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Technology Process of Ethyl-(10-(<(ethoxycarbonyl)methyl>thio)-7-phenyl-8-thia-6-azaspiro<4.5>deca-6.9-dien-9-carboxylat)

There total 3 articles about Ethyl-(10-(<(ethoxycarbonyl)methyl>thio)-7-phenyl-8-thia-6-azaspiro<4.5>deca-6.9-dien-9-carboxylat) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: 623-73-4
diazoacetic acid ethyl ester

: 122687-60-9
2-phenyl-3-thia-1-azaspiro[4,4]non-1-ene-4-thione

: 2-Phenyl-3-thia-1-azaspiro<4.4>non-1-en-4-on

: Ethyl-2-((4-(<(ethoxycarbonyl)methyl>thio)-2-phenyl-3-thia-1-azaspiro<4.4>non-1-en-4-yl)thio)acetat

: 158046-97-0
Ethyl-(10-(<(ethoxycarbonyl)methyl>thio)-7-phenyl-8-thia-6-azaspiro<4.5>deca-6.9-dien-9-carboxylat)

: (Z)-Ethyl-2-((4-(<(ethoxycarbonyl)(2-phenyl-3-thia-1-azaspiro<4.4>non-1-en-4-yliden)methyl>thio)-2-phenyl-3-thia-1-azaspiro<4.4>non-1-en-4-yl)thio)acetat

Guidance literature:: for 72h; Ambient temperature;
DOI:10.1002/hlca.19940770512

Reference yield: 9.3%

: 623-73-4
diazoacetic acid ethyl ester

: 122687-60-9
2-phenyl-3-thia-1-azaspiro[4,4]non-1-ene-4-thione

: 2-Phenyl-3-thia-1-azaspiro<4.4>non-1-en-4-on

: Ethyl-2-((4-(<(ethoxycarbonyl)methyl>thio)-2-phenyl-3-thia-1-azaspiro<4.4>non-1-en-4-yl)thio)acetat

: 158046-97-0
Ethyl-(10-(<(ethoxycarbonyl)methyl>thio)-7-phenyl-8-thia-6-azaspiro<4.5>deca-6.9-dien-9-carboxylat)

: (E)-Ethyl-2-((4-(<(ethoxycarbonyl)(2-phenyl-3-thia-1-azaspiro<4.4>non-1-en-4-yliden)methyl>thio)-2-phenyl-3-thia-1-azaspiro<4.4>non-1-en-4-yl)thio)acetat

Guidance literature:: In diethyl ether; for 72h; Ambient temperature;
DOI:10.1002/hlca.19940770512

Reference yield: 2.7%

: 623-73-4
diazoacetic acid ethyl ester

: 122687-60-9
2-phenyl-3-thia-1-azaspiro[4,4]non-1-ene-4-thione

: 2-Phenyl-3-thia-1-azaspiro<4.4>non-1-en-4-on

: Ethyl-(2-phenyl-3-thia-1-azaspiro<4.4>non-1-en-4-yliden)acetat

: Ethyl-2-((4-(<(ethoxycarbonyl)methyl>thio)-2-phenyl-3-thia-1-azaspiro<4.4>non-1-en-4-yl)thio)acetat

: 158046-97-0
Ethyl-(10-(<(ethoxycarbonyl)methyl>thio)-7-phenyl-8-thia-6-azaspiro<4.5>deca-6.9-dien-9-carboxylat)

: (E)-Ethyl-2-((4-(<(ethoxycarbonyl)(2-phenyl-3-thia-1-azaspiro<4.4>non-1-en-4-yliden)methyl>thio)-2-phenyl-3-thia-1-azaspiro<4.4>non-1-en-4-yl)thio)acetat

: (Z)-Ethyl-2-((4-(<(ethoxycarbonyl)(2-phenyl-3-thia-1-azaspiro<4.4>non-1-en-4-yliden)methyl>thio)-2-phenyl-3-thia-1-azaspiro<4.4>non-1-en-4-yl)thio)acetat

Guidance literature:: In diethyl ether; for 72h; Product distribution; Mechanism; Ambient temperature; or without solvent;
DOI:10.1002/hlca.19940770512