1-(2-azido-1-(4-(tert-butyl)phenyl)ethoxy)-2,2,6,6-tetramethylpiperidine

Base Information

Chemical Name:1-(2-azido-1-(4-(tert-butyl)phenyl)ethoxy)-2,2,6,6-tetramethylpiperidine
CAS No.:1449417-67-7
Molecular Formula:C₂₁H₃₄N₄O
Molecular Weight:358.527
Hs Code.:

Synonyms:1-(2-azido-1-(4-(tert-butyl)phenyl)ethoxy)-2,2,6,6-tetramethylpiperidine

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Chemical Property of 1-(2-azido-1-(4-(tert-butyl)phenyl)ethoxy)-2,2,6,6-tetramethylpiperidine

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Technology Process of 1-(2-azido-1-(4-(tert-butyl)phenyl)ethoxy)-2,2,6,6-tetramethylpiperidine

There total 3 articles about 1-(2-azido-1-(4-(tert-butyl)phenyl)ethoxy)-2,2,6,6-tetramethylpiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 2564-83-2,45842-10-2,126517-51-9,25657-03-8,26933-82-4,54637-06-8,64104-42-3
2,2,6,6-Tetramethyl-1-piperidinyloxy free radical

: 1746-23-2,26009-55-2
4-tert-Butylstyrene

: 1449417-67-7
1-(2-azido-1-(4-(tert-butyl)phenyl)ethoxy)-2,2,6,6-tetramethylpiperidine

Guidance literature:: With sodium azide; In water; acetonitrile; at 22 ℃; for 1.5h; Mechanism; Electrochemical reaction; Inert atmosphere;
DOI:10.1021/jacs.8b06744

Reference yield: 75.0%

: 1746-23-2,26009-55-2
4-tert-Butylstyrene

: 2,2,6,6-tetramethylpiperidine-1-oxoammonium tetrafluoroborate

: 1449417-67-7
1-(2-azido-1-(4-(tert-butyl)phenyl)ethoxy)-2,2,6,6-tetramethylpiperidine

Guidance literature:: With sodium azide; In acetonitrile; at 20 ℃; for 24h; under 760.051 Torr; Inert atmosphere;
DOI:10.1002/adsc.202100783

Reference yield:

: 2564-83-2
2,2,6,6-tetramethyl-piperidine-N-oxyl

: 1449417-67-7
1-(2-azido-1-(4-(tert-butyl)phenyl)ethoxy)-2,2,6,6-tetramethylpiperidine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium; naphthalene / tetrahydrofuran / 20 °C / Inert atmosphere

2: 1-azido-1λ³-benzo[d][1,2]iodaoxol-3(1H)-one / tetrahydrofuran; dichloromethane / 6 h / 20 °C / Inert atmosphere

With naphthalene; sodium; 1-azido-1λ³-benzo[d][1,2]iodaoxol-3(1H)-one; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol402106x