6-Iodo-2,3-dimethoxy-N-methoxymethyl-N-(6,7-methylenedioxy-1-naphthyl)benzamide

Base Information

Chemical Name:6-Iodo-2,3-dimethoxy-N-methoxymethyl-N-(6,7-methylenedioxy-1-naphthyl)benzamide
CAS No.:339267-21-9
Molecular Formula:C₂₂H₂₀INO₆
Molecular Weight:521.308
Hs Code.:

Synonyms:6-Iodo-2,3-dimethoxy-N-methoxymethyl-N-(6,7-methylenedioxy-1-naphthyl)benzamide

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Chemical Property of 6-Iodo-2,3-dimethoxy-N-methoxymethyl-N-(6,7-methylenedioxy-1-naphthyl)benzamide

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Technology Process of 6-Iodo-2,3-dimethoxy-N-methoxymethyl-N-(6,7-methylenedioxy-1-naphthyl)benzamide

There total 1 articles about 6-Iodo-2,3-dimethoxy-N-methoxymethyl-N-(6,7-methylenedioxy-1-naphthyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 107-30-2
chloromethyl methyl ether

: 181634-58-2
6-Iodo-2,3-dimethoxy-N-(6,7-methylenedioxy-1-naphthyl)benzamide

: 339267-21-9
6-Iodo-2,3-dimethoxy-N-methoxymethyl-N-(6,7-methylenedioxy-1-naphthyl)benzamide

Guidance literature:: 6-Iodo-2,3-dimethoxy-N-(6,7-methylenedioxy-1-naphthyl)benzamide; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

chloromethyl methyl ether; In N,N-dimethyl-formamide; at 20 ℃; for 2h; Further stages.;
DOI:10.1039/b008683p

Reference yield:

: 339267-21-9
6-Iodo-2,3-dimethoxy-N-methoxymethyl-N-(6,7-methylenedioxy-1-naphthyl)benzamide

: 6900-99-8
norchelerythrine

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / Na₂CO₃; PPh₃ / Pd(OAc)2 / dimethylformamide / 0.5 h / Heating

2: LAH / tetrahydrofuran / 0.5 h / 20 °C

3: 116 mg / aq. HCl / tetrahydrofuran / 1 h / 20 °C

With hydrogenchloride; lithium aluminium tetrahydride; sodium carbonate; triphenylphosphine; palladium diacetate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/b008683p