3,3-dimethylnorboranone ketal

Base Information

• Chemical Name: 3,3-dimethylnorboranone ketal
• CAS No.: 124287-80-5
• Molecular Formula: C₁₁H₂₀O₂
• Molecular Weight: 184.279
• Mol file: 124287-80-5.mol

Synonyms:3,3-dimethylnorboranone ketal

Chemical Property of 3,3-dimethylnorboranone ketal

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

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Technology Process of 3,3-dimethylnorboranone ketal

There total 2 articles about 3,3-dimethylnorboranone ketal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(+-)-camphenilone (13211-15-9) + 7,7-dimethylnorboranone ketal (124287-82-7) → camphor (514-15-8,32989-00-7) + 3,3-dimethylnorboranone ketal (124287-80-5)

Guidance literature:

With toluene-4-sulfonic acid; In 1,2-dimethoxyethane; for 2h; Equilibrium constant;

DOI:10.1021/jo00289a051

Reference yield:

(+-)-camphenilone (13211-15-9) + 2,2-dimethoxy-1,7,7-trimethylbicyclo<2.2.1>heptane (10395-50-3) → 1,7,7-trimethyl-bicyclo[2.2.1]heptan-2-one (736109-58-3,787517-91-3,68546-28-1) + 3,3-dimethylnorboranone ketal (124287-80-5)

Guidance literature:

With toluene-4-sulfonic acid; In 1,2-dimethoxyethane; for 2h; Equilibrium constant; other solvent;

DOI:10.1021/jo00289a051

Reference yield:

endo-3-methylbicyclo<2.2.1>heptan-2-one (3915-75-1,4154-60-3,100759-24-8,120410-05-1,131347-97-2,131726-05-1,131726-10-8,643-51-6) + 3,3-dimethylnorboranone ketal (124287-80-5) → (+-)-camphenilone (13211-15-9) + endo-3-methylnorboranone ketal (124287-79-2)

Guidance literature:

With toluene-4-sulfonic acid; In 1,2-dimethoxyethane; for 2h; Equilibrium constant; other solvent;

DOI:10.1021/jo00289a051

upstream raw materials:

(+-)-camphenilone

7,7-dimethylnorboranone ketal

2,2-dimethoxy-1,7,7-trimethylbicyclo<2.2.1>heptane

Downstream raw materials:

(+-)-camphenilone

endo-3-methylnorboranone ketal