endo-3-methylnorboranone ketal

Base Information

• Chemical Name: endo-3-methylnorboranone ketal
• CAS No.: 124287-79-2
• Molecular Formula: C₁₀H₁₈O₂
• Molecular Weight: 170.252
• Mol file: 124287-79-2.mol

Synonyms:endo-3-methylnorboranone ketal

Chemical Property of endo-3-methylnorboranone ketal

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of endo-3-methylnorboranone ketal

There total 2 articles about endo-3-methylnorboranone ketal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

endo-3-methylbicyclo<2.2.1>heptan-2-one (3915-75-1,4154-60-3,100759-24-8,120410-05-1,131347-97-2,131726-05-1,131726-10-8,643-51-6) + 3,3-dimethylnorboranone ketal (124287-80-5) → (+-)-camphenilone (13211-15-9) + endo-3-methylnorboranone ketal (124287-79-2)

Guidance literature:

With toluene-4-sulfonic acid; In 1,2-dimethoxyethane; for 2h; Equilibrium constant; other solvent;

DOI:10.1021/jo00289a051

Reference yield:

7,7-dimethylnorboranone ketal (124287-82-7) + endo-3-methylbicyclo<2.2.1>heptan-2-one (3915-75-1,4154-60-3,100759-24-8,120410-05-1,131347-97-2,131726-05-1,131726-10-8,643-51-6) → camphor (514-15-8,32989-00-7) + endo-3-methylnorboranone ketal (124287-79-2)

Guidance literature:

With toluene-4-sulfonic acid; In 1,2-dimethoxyethane; for 2h; Equilibrium constant; other solvent;

DOI:10.1021/jo00289a051

Reference yield:

Norbornan-2-on (497-38-1) + endo-3-methylnorboranone ketal (124287-79-2) → 2,2-dimethoxybicyclo<2.2.1>heptane (10395-51-4) + endo-3-methylbicyclo<2.2.1>heptan-2-one (3915-75-1,4154-60-3,100759-24-8,120410-05-1,131347-97-2,131726-05-1,131726-10-8,643-51-6)

Guidance literature:

With toluene-4-sulfonic acid; In 1,2-dimethoxyethane; for 2h; Equilibrium constant; other solvent;

DOI:10.1021/jo00289a051

upstream raw materials:

7,7-dimethylnorboranone ketal

endo-3-methylbicyclo<2.2.1>heptan-2-one

3,3-dimethylnorboranone ketal

Downstream raw materials:

2,2-dimethoxybicyclo<2.2.1>heptane

endo-3-methylbicyclo<2.2.1>heptan-2-one

Refernces