3-propanal

Base Information

Chemical Name:3-propanal
CAS No.:173440-72-7
Molecular Formula:C₁₉H₂₅NO₇
Molecular Weight:379.41
Hs Code.:

3-<benzyloxycarbonyl-4-(3-methoxymethoxypropyl)-5-oxo-1,3-oxazolidin-4-yl>propanal

Synonyms:3-propanal

Suppliers and Price of 3-propanal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-propanal

Chemical Property:

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Technology Process of 3-propanal

There total 3 articles about 3-propanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.5%

: 173440-71-6
3-(benzyloxycarbonyl)-4-(3-hydroxypropyl)-4-(3-methoxymethoxypropyl)-1,3-oxazolidin-5-one

: 173440-72-7
3-propanal

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -60 ℃; for 0.25h;
DOI:10.1248/cpb.43.1683

Reference yield:

: 23632-67-9
(S)-3-[3-(benzyloxycarbonyl)-5-oxooxazolidin-4-yl]propanoic acid

: 173440-72-7
3-propanal

Guidance literature:: Multi-step reaction with 5 steps

1: 83.8 percent / BH₃*THF / tetrahydrofuran / 20 h / 4 °C

2: 52.7 percent / diisopropylethylamine / CH₂Cl₂ / 2 h

3: 1.) potassium bis(trimethylsilyl)amide / 1.) THF, toluene, -78 deg C, 3 min, 2.) THF, toluene, -78 deg C, 20 min

4: 1.) 9-borabicyclo<3.3.1>nonane, 2.) 30percent aq. H₂O₂, 2N aq. NaOH / 1.) THF, 14 h, 2.) THF, 1 h

5: 97.5 percent / DMSO, oxalyl chloride / CH₂Cl₂ / 0.25 h / -60 °C

With sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; borane-THF; oxalyl dichloride; dihydrogen peroxide; potassium hexamethylsilazane; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1248/cpb.43.1683

Reference yield:

: 173440-70-5
3-(benzyloxycarbonyl)-4-(3-methoxymethoxypropyl)-4-(2-propenyl)-1,3-oxazolidin-5-one

: 173440-72-7
3-propanal

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 9-borabicyclo<3.3.1>nonane, 2.) 30percent aq. H₂O₂, 2N aq. NaOH / 1.) THF, 14 h, 2.) THF, 1 h

2: 97.5 percent / DMSO, oxalyl chloride / CH₂Cl₂ / 0.25 h / -60 °C

With sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; oxalyl dichloride; dihydrogen peroxide; dimethyl sulfoxide; In dichloromethane;
DOI:10.1248/cpb.43.1683