N,N'-(2,4,6-triethyl-1,3-phenylene)bis(methylene)bis(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluorononanamide)

Base Information

• Chemical Name: N,N'-(2,4,6-triethyl-1,3-phenylene)bis(methylene)bis(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluorononanamide)
• CAS No.: 1137672-93-5
• Molecular Formula: C₃₂H₃₀F₂₆N₂O₂
• Molecular Weight: 968.561

Synonyms:N,N'-(2,4,6-triethyl-1,3-phenylene)bis(methylene)bis(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluorononanamide)

Chemical Property of N,N'-(2,4,6-triethyl-1,3-phenylene)bis(methylene)bis(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluorononanamide)

Chemical Property:

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Technology Process of N,N'-(2,4,6-triethyl-1,3-phenylene)bis(methylene)bis(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluorononanamide)

There total 1 articles about N,N'-(2,4,6-triethyl-1,3-phenylene)bis(methylene)bis(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluorononanamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluorononanoic acid (27854-30-4) + 1,3-bis-(aminomethyl)-2,4,6,-triethylbenzene → N,N'-(2,4,6-triethyl-1,3-phenylene)bis(methylene)bis(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluorononanamide) (1137672-93-5)

Guidance literature:

With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 60 ℃; for 3h; Inert atmosphere;

DOI:10.1021/jo9000788

Reference yield:

N,N'-(2,4,6-triethyl-1,3-phenylene)bis(methylene)bis(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluorononanamide) (1137672-93-5) + tetraethylammonium chloride (56-34-8) → C8H20N(1+)*C32H30F26N2O2*Cl(1-)

Guidance literature:

In chloroform-d1; at 21.84 ℃;

DOI:10.1021/jo9000788

Reference yield:

N,N'-(2,4,6-triethyl-1,3-phenylene)bis(methylene)bis(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluorononanamide) (1137672-93-5) + tetraethylammonium tosylate (733-44-8) → C7H7O3S(1-)*C8H20N(1+)*C32H30F26N2O2

Guidance literature:

In chloroform-d1; at 21.84 ℃;

DOI:10.1021/jo9000788

upstream raw materials:

4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluorononanoic acid

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