N⁽¹⁾,N⁽¹⁾'-((naphthalene-2,7-diylbis(azanediyl))bis(2-oxoethane-2,1-diyl))bis(N⁽³⁾-(2-ethylhexyl)-4,6-bis((2-ethylhexyl)oxy)isophthalamide)

Base Information

• Chemical Name: N⁽¹⁾,N⁽¹⁾'-((naphthalene-2,7-diylbis(azanediyl))bis(2-oxoethane-2,1-diyl))bis(N⁽³⁾-(2-ethylhexyl)-4,6-bis((2-ethylhexyl)oxy)isophthalamide)
• CAS No.: 1260632-55-0
• Molecular Formula: C₇₈H₁₂₂N₆O₁₀
• Molecular Weight: 1303.86

Synonyms:N⁽¹⁾,N⁽¹⁾'-((naphthalene-2,7-diylbis(azanediyl))bis(2-oxoethane-2,1-diyl))bis(N⁽³⁾-(2-ethylhexyl)-4,6-bis((2-ethylhexyl)oxy)isophthalamide)

Chemical Property of N⁽¹⁾,N⁽¹⁾'-((naphthalene-2,7-diylbis(azanediyl))bis(2-oxoethane-2,1-diyl))bis(N⁽³⁾-(2-ethylhexyl)-4,6-bis((2-ethylhexyl)oxy)isophthalamide)

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Technology Process of N⁽¹⁾,N⁽¹⁾'-((naphthalene-2,7-diylbis(azanediyl))bis(2-oxoethane-2,1-diyl))bis(N⁽³⁾-(2-ethylhexyl)-4,6-bis((2-ethylhexyl)oxy)isophthalamide)

There total 3 articles about N⁽¹⁾,N⁽¹⁾'-((naphthalene-2,7-diylbis(azanediyl))bis(2-oxoethane-2,1-diyl))bis(N⁽³⁾-(2-ethylhexyl)-4,6-bis((2-ethylhexyl)oxy)isophthalamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

2-(5-((2-ethylhexyl)carbamoyl)-2,4-bis((2-ethylhexyl)oxy)benzamido)acetic acid (1260632-44-7) + 2,7-diaminonaphthalene (613-76-3) → N(1),N(1)'-((naphthalene-2,7-diylbis(azanediyl))bis(2-oxoethane-2,1-diyl))bis(N(3)-(2-ethylhexyl)-4,6-bis((2-ethylhexyl)oxy)isophthalamide) (1260632-55-0)

Guidance literature:

2-(5-((2-ethylhexyl)carbamoyl)-2,4-bis((2-ethylhexyl)oxy)benzamido)acetic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; for 2h; Inert atmosphere;

2,7-diaminonaphthalene; In dichloromethane; at 20 ℃; for 30h; Inert atmosphere; Reflux;

DOI:10.1021/ol102522m

Reference yield:

C36H62N2O6 → N(1),N(1)'-((naphthalene-2,7-diylbis(azanediyl))bis(2-oxoethane-2,1-diyl))bis(N(3)-(2-ethylhexyl)-4,6-bis((2-ethylhexyl)oxy)isophthalamide) (1260632-55-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: water; sodium hydroxide / methanol / 6 h

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 2 h / Inert atmosphere

2.2: 30 h / 20 °C / Inert atmosphere; Reflux

With water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In methanol; dichloromethane;

DOI:10.1021/ol102522m

Reference yield:

5-((2-ethylhexyl)carbamoyl)-2,4-bis((2-ethylhexyl)oxy)benzoic acid (1260632-42-5) → N(1),N(1)'-((naphthalene-2,7-diylbis(azanediyl))bis(2-oxoethane-2,1-diyl))bis(N(3)-(2-ethylhexyl)-4,6-bis((2-ethylhexyl)oxy)isophthalamide) (1260632-55-0)

Guidance literature:

Multi-step reaction with 3 steps

1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 2 h / Inert atmosphere

1.2: 24 h / Inert atmosphere

2.1: water; sodium hydroxide / methanol / 6 h

3.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 2 h / Inert atmosphere

3.2: 30 h / 20 °C / Inert atmosphere; Reflux

With water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In methanol; dichloromethane;

DOI:10.1021/ol102522m

upstream raw materials:

5-((2-ethylhexyl)carbamoyl)-2,4-bis((2-ethylhexyl)oxy)benzoic acid

2-(5-((2-ethylhexyl)carbamoyl)-2,4-bis((2-ethylhexyl)oxy)benzamido)acetic acid

2,7-diaminonaphthalene

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