Technology Process of C60H66F3NO18
There total 5 articles about C60H66F3NO18 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
dichloromethane; water;
Ambient temperature;
DOI:10.1016/S0008-6215(96)00275-3
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 99 percent / NaH / dimethylformamide / 1.33 h
2: 89 percent / 1) 4 Angstroem molecular sieves, 2) dimethyl(methylthio)sulfonium triflate / diethyl ether / 1) 1 h, 2) 0 deg C, 10 min; room temperature, 30 min
3: 84 percent / DDQ / CH2Cl2; H2O / Ambient temperature
With
4 A molecular sieve; sodium hydride; dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
diethyl ether; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(96)00275-3
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 76 percent / 1) 4 Angstroem molecular sieves, 2) trimethylsilyl trifluoromethanesulfonate / nitromethane / 1) 0 deg C, 1 h, 2) 1.5 h
2: 90 percent / NaOMe / methanol / 1.5 h / Ambient temperature
3: 99 percent / NaH / dimethylformamide / 1.33 h
4: 89 percent / 1) 4 Angstroem molecular sieves, 2) dimethyl(methylthio)sulfonium triflate / diethyl ether / 1) 1 h, 2) 0 deg C, 10 min; room temperature, 30 min
5: 84 percent / DDQ / CH2Cl2; H2O / Ambient temperature
With
trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; sodium methylate; sodium hydride; dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
methanol; diethyl ether; nitromethane; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(96)00275-3
