Benzeneethanol, beta-bromo-alpha-phenyl-, 1-formate

Base Information

• Chemical Name: Benzeneethanol, beta-bromo-alpha-phenyl-, 1-formate
• CAS No.: 134510-09-1
• Molecular Formula: C₁₅H₁₃BrO₂
• Molecular Weight: 305.171
• DSSTox Substance ID: DTXSID701256528
• Nikkaji Number: J1.093.265C
• Mol file: 134510-09-1.mol

Synonyms:DTXSID701256528;134510-09-1

Chemical Property of Benzeneethanol, beta-bromo-alpha-phenyl-, 1-formate

Chemical Property:

• XLogP3: 3.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 5
• Exact Mass: 304.00989
• Heavy Atom Count: 18
• Complexity: 245

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C(C(C2=CC=CC=C2)Br)OC=O

Technology Process of Benzeneethanol, beta-bromo-alpha-phenyl-, 1-formate

There total 1 articles about Benzeneethanol, beta-bromo-alpha-phenyl-, 1-formate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

stilbene (588-59-0) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 2-bromo-1,2-diphenylethyl formate (134510-09-1)

Guidance literature:

stilbene; N,N-dimethyl-formamide; With dibromamine-T; at 20 ℃; for 0.166667h; Inert atmosphere;

With water; for 0.25h;

DOI:10.1016/j.tetlet.2011.11.138

Reference yield: 80.0%

2-bromo-1,2-diphenylethyl formate (134510-09-1) → benzil (134-81-6)

Guidance literature:

With hydrogen bromide; dimethyl sulfoxide; at 115 ℃; for 4h;

DOI:10.1007/BF00958570

upstream raw materials:

stilbene

N,N-dimethyl-formamide

Downstream raw materials:

benzil