3-(2-(4-methoxybenzoyl)-thiophenyl)-3,4,5-tri-O-acetyl-β-D-glucuronic acid methyl ester

Base Information

Chemical Name:3-(2-(4-methoxybenzoyl)-thiophenyl)-3,4,5-tri-O-acetyl-β-D-glucuronic acid methyl ester
CAS No.:1215169-55-3
Molecular Formula:C₂₅H₂₆O₁₂S
Molecular Weight:550.54
Hs Code.:

Synonyms:3-(2-(4-methoxybenzoyl)-thiophenyl)-3,4,5-tri-O-acetyl-β-D-glucuronic acid methyl ester

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Chemical Property of 3-(2-(4-methoxybenzoyl)-thiophenyl)-3,4,5-tri-O-acetyl-β-D-glucuronic acid methyl ester

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Technology Process of 3-(2-(4-methoxybenzoyl)-thiophenyl)-3,4,5-tri-O-acetyl-β-D-glucuronic acid methyl ester

There total 1 articles about 3-(2-(4-methoxybenzoyl)-thiophenyl)-3,4,5-tri-O-acetyl-β-D-glucuronic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

(3-hydroxythiophen-2-yl)-(4-methoxyphenyl)-methanone: 647833-71-4
(3-hydroxythiophen-2-yl)-(4-methoxyphenyl)-methanone

: 21085-72-3
1-bromo-2,3,4-tri-O-acetyl-α-D-glucuronic acid methyl ester

: 1215169-55-3
3-(2-(4-methoxybenzoyl)-thiophenyl)-3,4,5-tri-O-acetyl-β-D-glucuronic acid methyl ester

Guidance literature:: (3-hydroxythiophen-2-yl)-(4-methoxyphenyl)-methanone; 1-bromo-2,3,4-tri-O-acetyl-α-D-glucuronic acid methyl ester; With tetrabutylammomium bromide; potassium carbonate; In dichloromethane; water; at 20 ℃; for 24h; Inert atmosphere;

With silver carbonate; In dichloromethane; water; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2009.12.003

Reference yield: 92.0%

: 1215169-55-3
3-(2-(4-methoxybenzoyl)-thiophenyl)-3,4,5-tri-O-acetyl-β-D-glucuronic acid methyl ester

: 1215169-56-4
3-(2-(4-methoxybenzyl)-thiophenyl)-β-D-glucuronic methyl ester

Guidance literature:: 3-(2-(4-methoxybenzoyl)-thiophenyl)-3,4,5-tri-O-acetyl-β-D-glucuronic acid methyl ester; With sodium cyanoborohydride; In acetonitrile; at 0 ℃; for 0.5h; Inert atmosphere;

With chloro-trimethyl-silane; In acetonitrile; at 0 - 4 ℃; Inert atmosphere;

With water; sodium hydrogencarbonate; In acetonitrile; at 5 ℃; for 0.0833333h; Inert atmosphere;
DOI:10.1016/j.tet.2009.12.003