methyl (2E)-3-[2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]acrylate

Base Information

Chemical Name:methyl (2E)-3-[2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]acrylate
CAS No.:372193-92-5
Molecular Formula:C₁₆H₂₁BO₄
Molecular Weight:288.151
Hs Code.:

Synonyms:methyl (2E)-3-[2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]acrylate

Suppliers and Price of methyl (2E)-3-[2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]acrylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of methyl (2E)-3-[2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]acrylate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of methyl (2E)-3-[2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]acrylate

There total 3 articles about methyl (2E)-3-[2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 21204-67-1,2605-67-6
methyl (triphenylphosphoranylidene)acetate

: 380151-85-9
2-(2'-formylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 372193-92-5
methyl (2E)-3-[2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]acrylate

: methyl (2Z)-3-[2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]acrylate

Guidance literature:: In toluene; at 90 ℃; for 18h;
DOI:10.1021/jo049874k

Reference yield:

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 372193-92-5
methyl (2E)-3-[2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]acrylate

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / benzene / 5 h / Heating

2: 87 percent / toluene / 18 h / 90 °C

In toluene; benzene; 2: Wittig reaction;
DOI:10.1021/jo049874k

Reference yield:

: 40138-16-7
2-formylbenzene boronic acid

: 372193-92-5
methyl (2E)-3-[2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]acrylate

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / benzene / 5 h / Heating

2: 87 percent / toluene / 18 h / 90 °C

In toluene; benzene; 2: Wittig reaction;
DOI:10.1021/jo049874k