1N-(3'-C-allyl-3'-O-benzyl-5'-O-trityl-2'-deoxy-β-D-xylofuranosyl)thymine

Base Information

Chemical Name:1N-(3'-C-allyl-3'-O-benzyl-5'-O-trityl-2'-deoxy-β-D-xylofuranosyl)thymine
CAS No.:1112393-13-1
Molecular Formula:C₃₉H₃₈N₂O₅
Molecular Weight:614.741
Hs Code.:

Synonyms:1N-(3'-C-allyl-3'-O-benzyl-5'-O-trityl-2'-deoxy-β-D-xylofuranosyl)thymine

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Chemical Property of 1N-(3'-C-allyl-3'-O-benzyl-5'-O-trityl-2'-deoxy-β-D-xylofuranosyl)thymine

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Technology Process of 1N-(3'-C-allyl-3'-O-benzyl-5'-O-trityl-2'-deoxy-β-D-xylofuranosyl)thymine

There total 1 articles about 1N-(3'-C-allyl-3'-O-benzyl-5'-O-trityl-2'-deoxy-β-D-xylofuranosyl)thymine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1112393-11-9
1-N-(3'-C-allyl-5'-O-trityl-2'-deoxy-β-D-xylofuranosyl)thymine

: 100-39-0
benzyl bromide

: 1112393-13-1
1N-(3'-C-allyl-3'-O-benzyl-5'-O-trityl-2'-deoxy-β-D-xylofuranosyl)thymine

: 1112393-16-4
1N-(3'-C-allyl-3'-O-benzyl-5'-O-trityl-2'-deoxy-β-D-xylofuranosyl)-3N-benzylthymine

Guidance literature:: 1-N-(3'-C-allyl-5'-O-trityl-2'-deoxy-β-D-xylofuranosyl)thymine; With sodium hydride; In tetrahydrofuran; oil; at -78 ℃; for 1h; Inert atmosphere;

benzyl bromide; In tetrahydrofuran; oil; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1021/jo8023472

Reference yield: 75.0%

: 1112393-13-1
1N-(3'-C-allyl-3'-O-benzyl-5'-O-trityl-2'-deoxy-β-D-xylofuranosyl)thymine

: 1112393-18-6
1N-(3'-C-allyl-3'-O-benzyl-2'-deoxy-β-D-xylofuranosyl)thymine

Guidance literature:: 1N-(3'-C-allyl-3'-O-benzyl-5'-O-trityl-2'-deoxy-β-D-xylofuranosyl)thymine; With water; acetic acid; at 90 ℃; for 6h;

With sodium methylate; In methanol; at 20 ℃; for 17h; Inert atmosphere;
DOI:10.1021/jo8023472