(S)-1-(4-methoxybenzyl)-5-(1-((tributylstannyl)methoxy)ethyl)-1,2,3,6-tetrahydropyridine

Base Information

Chemical Name:(S)-1-(4-methoxybenzyl)-5-(1-((tributylstannyl)methoxy)ethyl)-1,2,3,6-tetrahydropyridine
CAS No.:1383568-86-2
Molecular Formula:C₂₈H₄₉NO₂Sn
Molecular Weight:550.413
Hs Code.:

Synonyms:(S)-1-(4-methoxybenzyl)-5-(1-((tributylstannyl)methoxy)ethyl)-1,2,3,6-tetrahydropyridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-1-(4-methoxybenzyl)-5-(1-((tributylstannyl)methoxy)ethyl)-1,2,3,6-tetrahydropyridine

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Technology Process of (S)-1-(4-methoxybenzyl)-5-(1-((tributylstannyl)methoxy)ethyl)-1,2,3,6-tetrahydropyridine

There total 4 articles about (S)-1-(4-methoxybenzyl)-5-(1-((tributylstannyl)methoxy)ethyl)-1,2,3,6-tetrahydropyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1312678-77-5
(S)-1-(N-(4-methoxybenzyl)-1,2,5,6-tetrahydropyridin-3-yl)ethanol

: 66222-29-5
tri-n-butylstannylmethyl iodide

: 1383568-86-2
(S)-1-(4-methoxybenzyl)-5-(1-((tributylstannyl)methoxy)ethyl)-1,2,3,6-tetrahydropyridine

Guidance literature:: (S)-1-(N-(4-methoxybenzyl)-1,2,5,6-tetrahydropyridin-3-yl)ethanol; With potassium hydride; In tetrahydrofuran; at 20 ℃; for 1h;

tri-n-butylstannylmethyl iodide; In tetrahydrofuran; at 20 ℃; for 4h;

Reference yield:

: 4754-27-2
1-(3-Pyridyl)ethanol

: 1383568-86-2
(S)-1-(4-methoxybenzyl)-5-(1-((tributylstannyl)methoxy)ethyl)-1,2,3,6-tetrahydropyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 1,2-dichloro-ethane / Reflux

2: Amano Lipase PS / hexane / 18 h / Molecular sieve; Resolution of racemate; Enzymatic reaction

3: potassium hydride / tetrahydrofuran

With Amano Lipase PS; potassium hydride; In tetrahydrofuran; hexane; 1,2-dichloro-ethane;
DOI:10.1038/nchem.1050

Reference yield:

: 1312678-79-7
(+/-)-1-(N-(4-methoxybenzyl)-1,2,5,6-tetrahydropyridin-3-yl)ethanol

: 1383568-86-2
(S)-1-(4-methoxybenzyl)-5-(1-((tributylstannyl)methoxy)ethyl)-1,2,3,6-tetrahydropyridine

Guidance literature:: Multi-step reaction with 2 steps

1: Amano Lipase PS / hexane / 18 h / Molecular sieve; Resolution of racemate; Enzymatic reaction

2: potassium hydride / tetrahydrofuran

With Amano Lipase PS; potassium hydride; In tetrahydrofuran; hexane;
DOI:10.1038/nchem.1050