C₃₁SiH₄₀O₄

Base Information

Chemical Name:C₃₁SiH₄₀O₄
CAS No.:250577-77-6
Molecular Formula:C₃₁H₄₀O₄Si
Molecular Weight:504.742
Hs Code.:

C<sub>31</sub>SiH<sub>40</sub>O<sub>4</sub>

Synonyms:C₃₁SiH₄₀O₄

Suppliers and Price of C₃₁SiH₄₀O₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₁SiH₄₀O₄

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₁SiH₄₀O₄

There total 1 articles about C₃₁SiH₄₀O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: ethyl (3S)-3-hydroxy-4-O-triphenylmethyloxybutanoate

: 18162-48-6
tert-butyldimethylsilyl chloride

: 250577-77-6
C₃₁SiH₄₀O₄

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;
DOI:10.1021/ol990281j

Reference yield:

: 250577-77-6
C₃₁SiH₄₀O₄

: C₃₁H₅₀O₇Si

Guidance literature:: Multi-step reaction with 15 steps

1.1: 75 percent / H₂ / Pd/C / ethanol / 24 h / 2068.65 Torr

2.1: dimethyl sulfoxide; oxalyl chloride; ethyldiisopropylamine / CH₂Cl₂ / 0.92 h / -78 - 20 °C

3.1: 3.39 g / toluene / 1 h / 70 °C

4.1: sodium hexamethyldisilazide / tetrahydrofuran / 0 - 20 °C

4.2: 82 percent / tetrahydrofuran / 0.58 h / -78 - 20 °C

5.1: 73 percent / diisobutylaluminum hydride / CH₂Cl₂; hexane / -78 - 0 °C

6.1: triethylamine / CH₂Cl₂ / 0 - 20 °C

7.1: 3.53 g / sodium iodide / acetone / 2 h / Heating

8.1: 98 percent / benzene / 14 h / Heating

9.1: sodium hexamethyldisilazide / tetrahydrofuran / 1 h / -78 °C

9.2: 78 percent / tetrahydrofuran / -78 - 20 °C

10.1: 90 mg / benzene; CH₂Cl₂ / 120 h / 20 °C

11.1: 99 percent / diisobutylaluminum hydride / CH₂Cl₂; toluene / 0.08 h / -78 °C

12.1: triethylamine / CH₂Cl₂ / 0 - 20 °C

13.1: 126 mg / sodium iodide / acetone / 1 h / Heating

14.1: hydrazine monohydrate; 1-hexene / ethanol / 1 h / 40 °C

15.1: 19 mg / air; 1-hexene / CH₂Cl₂ / 3 h

With 1-hexene; oxalyl dichloride; air; hydrogen; sodium hexamethyldisilazane; diisobutylaluminium hydride; hydrazine hydrate; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; sodium iodide; palladium on activated charcoal; In tetrahydrofuran; ethanol; hexane; dichloromethane; acetone; toluene; benzene; 2.1: Swern oxidation / 3.1: Wittig olefination / 4.2: Wittig olefination / 10.1: Wittig olefination;
DOI:10.1021/ol990281j

Reference yield:

: 250577-77-6
C₃₁SiH₄₀O₄

: 250577-76-5
C₃₂H₅₀O₉Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: 75 percent / H₂ / Pd/C / ethanol / 24 h / 2068.65 Torr

2.1: dimethyl sulfoxide; oxalyl chloride; ethyldiisopropylamine / CH₂Cl₂ / 0.92 h / -78 - 20 °C

3.1: 3.39 g / toluene / 1 h / 70 °C

4.1: sodium hexamethyldisilazide / tetrahydrofuran / 0 - 20 °C

4.2: 82 percent / tetrahydrofuran / 0.58 h / -78 - 20 °C

5.1: 73 percent / diisobutylaluminum hydride / CH₂Cl₂; hexane / -78 - 0 °C

6.1: triethylamine / CH₂Cl₂ / 0 - 20 °C

7.1: 3.53 g / sodium iodide / acetone / 2 h / Heating

8.1: 98 percent / benzene / 14 h / Heating

9.1: sodium hexamethyldisilazide / tetrahydrofuran / 1 h / -78 °C

9.2: 78 percent / tetrahydrofuran / -78 - 20 °C

10.1: 90 mg / benzene; CH₂Cl₂ / 120 h / 20 °C

With oxalyl dichloride; hydrogen; sodium hexamethyldisilazane; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; sodium iodide; palladium on activated charcoal; In tetrahydrofuran; ethanol; hexane; dichloromethane; acetone; toluene; benzene; 2.1: Swern oxidation / 3.1: Wittig olefination / 4.2: Wittig olefination / 10.1: Wittig olefination;
DOI:10.1021/ol990281j