C₁₅H₁₀Cl₂F₂N₂OS

Base Information

Chemical Name:C₁₅H₁₀Cl₂F₂N₂OS
CAS No.:1372148-86-1
Molecular Formula:C₁₅H₁₀Cl₂F₂N₂OS
Molecular Weight:375.226
Hs Code.:

C<sub>15</sub>H<sub>10</sub>Cl<sub>2</sub>F<sub>2</sub>N<sub>2</sub>OS

Synonyms:C₁₅H₁₀Cl₂F₂N₂OS

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₁₀Cl₂F₂N₂OS

Chemical Property:

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Technology Process of C₁₅H₁₀Cl₂F₂N₂OS

There total 1 articles about C₁₅H₁₀Cl₂F₂N₂OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 412018-50-9
1-(4,6-dichloropyridin-3-yl)ethan-1-one

: 141106-52-7
2,4-difluorophenyl isothiocyanate

: 74-88-4
methyl iodide

: 1372148-86-1
C₁₅H₁₀Cl₂F₂N₂OS

Guidance literature:: 1-(4,6-dichloropyridin-3-yl)ethan-1-one; With lithium diisopropyl amide; In tetrahydrofuran; at -40 ℃; for 0.5h; Inert atmosphere;

2,4-difluorophenyl isothiocyanate; In tetrahydrofuran; at -40 - 20 ℃; for 1.5h;

methyl iodide; In tetrahydrofuran; at 5 - 20 ℃; for 0.333333h;
DOI:10.1055/s-0031-1290079

Reference yield: 94.0%

: 1372148-86-1
C₁₅H₁₀Cl₂F₂N₂OS

: 1372148-87-2
C₁₅H₉ClF₂N₂OS

Guidance literature:: With potassium phosphate; In dimethyl sulfoxide; at 100 ℃; for 0.5h;
DOI:10.1055/s-0031-1290079

Reference yield:

: 1372148-86-1
C₁₅H₁₀Cl₂F₂N₂OS

: 1372148-91-8
C₂₀H₁₅F₂N₃O₄S

Guidance literature:: Multi-step reaction with 3 steps

1: potassium phosphate / dimethyl sulfoxide / 0.5 h / 100 °C

2: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; triethylamine / 1,4-dioxane / 5 h / Reflux

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 21 h / 20 °C

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; palladium diacetate; triethylamine; 3-chloro-benzenecarboperoxoic acid; In 1,4-dioxane; dichloromethane; dimethyl sulfoxide; 2: Suzuki-Miyaura coupling;
DOI:10.1055/s-0031-1290079