Technology Process of 8-(3-tolyl)-7,9-diphenyl-8H-acenaphtho[1,2-c]pyrrole
There total 3 articles about 8-(3-tolyl)-7,9-diphenyl-8H-acenaphtho[1,2-c]pyrrole which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine; palladium dichloride;
In
dimethyl sulfoxide;
at 100 ℃;
for 8h;
Under air;
DOI:10.1002/chem.201101483
- Guidance literature:
-
Multi-step reaction with 2 steps
1: copper(l) iodide; bis(triphenylphosphine)palladium(II)-chloride; triethylamine; triphenylphosphine / 10 h / 20 - 50 °C / Inert atmosphere
2: triethylamine; palladium dichloride / dimethyl sulfoxide / 8 h / 100 °C / Under air
With
copper(l) iodide; bis(triphenylphosphine)palladium(II)-chloride; triethylamine; triphenylphosphine; palladium dichloride;
In
dimethyl sulfoxide;
1: Sonogashira coupling;
DOI:10.1002/chem.201101483
- Guidance literature:
-
Multi-step reaction with 2 steps
1: copper(l) iodide; bis(triphenylphosphine)palladium(II)-chloride; triethylamine; triphenylphosphine / 10 h / 20 - 50 °C / Inert atmosphere
2: triethylamine; palladium dichloride / dimethyl sulfoxide / 8 h / 100 °C / Under air
With
copper(l) iodide; bis(triphenylphosphine)palladium(II)-chloride; triethylamine; triphenylphosphine; palladium dichloride;
In
dimethyl sulfoxide;
1: Sonogashira coupling;
DOI:10.1002/chem.201101483
