1,3,4,6-tetra-O-acetyl-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside

Base Information

• Chemical Name: 1,3,4,6-tetra-O-acetyl-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside
• CAS No.: 82264-19-5
• Molecular Formula: C₂₂H₂₇NO₁₁
• Molecular Weight: 481.456

Synonyms:1,3,4,6-tetra-O-acetyl-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside

Chemical Property of 1,3,4,6-tetra-O-acetyl-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,3,4,6-tetra-O-acetyl-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside

There total 9 articles about 1,3,4,6-tetra-O-acetyl-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

benzyl chloroformate (501-53-1,94274-21-2) + acetyl 3,4,6-tri-O-acetyl-2-amino-2-deoxy-D-glucopyranoside hydrochloride (5432-46-2,1191127-63-5) → 1,3,4,6-tetra-O-acetyl-2-deoxy-2-(benzyloxycarbonyl)amino-α/β-D-glucopyranoside (5348-99-2,35946-66-8,82264-19-5,100483-05-4)

Guidance literature:

With sodium hydrogencarbonate; In dichloromethane; water; at 20 ℃; pH=9;

DOI:10.1002/chem.202005228

Reference yield: 94.0%

2-carbobenzyloxyamino-2-deoxy-D-glucopyranose (3006-58-4,13030-01-8,42890-10-8,42973-23-9,77059-32-6,121785-09-9,7474-40-0) + acetic anhydride (108-24-7) → 1,3,4,6-tetra-O-acetyl-2-deoxy-2-(benzyloxycarbonyl)amino-α/β-D-glucopyranoside (5348-99-2,35946-66-8,82264-19-5,100483-05-4)

Guidance literature:

With toluene-4-sulfonic acid; In acetonitrile; at 0 - 40 ℃; for 3h;

DOI:10.1016/j.carres.2008.01.014

Reference yield: 70.0%

2-carbobenzyloxyamino-2-deoxy-D-glucopyranose (3006-58-4,13030-01-8,42890-10-8,42973-23-9,77059-32-6,121785-09-9,7474-40-0) + acetic anhydride (108-24-7) → 2-(acetoxymethyl)-5-{[(benzyloxy)carbonyl]amino}tetrahydropyran-3,4,6-triyl triacetate (35946-66-8) + 1,3,4,6-tetra-O-acetyl-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside (82264-19-5)

Guidance literature:

With sodium acetate; at 85 ℃; for 3h;

DOI:10.1021/ja00380a019

upstream raw materials:

2-benzyloxycarbonylamino-2-deoxy-D-glucose

2-carbobenzyloxyamino-2-deoxy-D-glucopyranose

acetic anhydride

D-glucosamine hydrochloride

Downstream raw materials:

2-benzyloxycarbonylamino-2-deoxy-3,4,6-tri-O-acetyl-D-glucopyranose

3,4,6,7-tetra-O-benzyl-1-deoxy-α-D-gluco-hept-2-ulopyranosyl-(2-1)-3,4,6-tri-O-acetyl-2-deoxy-2-benzylcarbamate-β-D-glucopyranoside

3,4,6,7-tetra-O-benzyl-1-deoxy-α-D-gluco-hept-2-ulopyranosyl-(2-1)-3,4,6-tri-O-acetyl-2-deoxy-2-benzylcarbamate-α-D-glucopyranoside

C₄₉H₅₅NO₁₂

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 82264-19-5 1,3,4,6-tetra-O-acetyl-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside

Send

Send

Metric Ton KG G Pound L ML

Send

Send