3-(tert-Butyldimethylsilyl)oxy-N-(2-iodophenyl)-N,4,4-trimethylpentanamide

Base Information

Chemical Name:3-(tert-Butyldimethylsilyl)oxy-N-(2-iodophenyl)-N,4,4-trimethylpentanamide
CAS No.:150983-07-6
Molecular Formula:C₂₀H₃₄INO₂Si
Molecular Weight:475.485
Hs Code.:

Synonyms:3-(tert-Butyldimethylsilyl)oxy-N-(2-iodophenyl)-N,4,4-trimethylpentanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(tert-Butyldimethylsilyl)oxy-N-(2-iodophenyl)-N,4,4-trimethylpentanamide

Chemical Property:

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Technology Process of 3-(tert-Butyldimethylsilyl)oxy-N-(2-iodophenyl)-N,4,4-trimethylpentanamide

There total 4 articles about 3-(tert-Butyldimethylsilyl)oxy-N-(2-iodophenyl)-N,4,4-trimethylpentanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 69739-34-0
t-butyldimethylsiyl triflate

: 135190-94-2
3-Hydroxy-4,4-dimethyl-pentanoic acid (2-iodo-phenyl)-methyl-amide

: 150983-07-6
3-(tert-Butyldimethylsilyl)oxy-N-(2-iodophenyl)-N,4,4-trimethylpentanamide

Guidance literature:: at 25 ℃; for 23.5h;
DOI:10.1016/S0040-4020(01)80401-4

Reference yield:

: 57056-93-6
N-methyl-2-iodoaniline

: 150983-07-6
3-(tert-Butyldimethylsilyl)oxy-N-(2-iodophenyl)-N,4,4-trimethylpentanamide

Guidance literature:: Multi-step reaction with 3 steps

1: 8.5 M NaOH / tetrahydrofuran / 1) 0 deg C, 30 min, 2) 25 deg C, 3 h

2: 96 percent / LDA / tetrahydrofuran / 0.08 h / -78 °C

3: 100 percent / 23.5 h / 25 °C

With sodium hydroxide; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1016/S0040-4020(01)80401-4

Reference yield:

: 90585-26-5
N-(2-iodophenyl)-N-methylacetamide

: 150983-07-6
3-(tert-Butyldimethylsilyl)oxy-N-(2-iodophenyl)-N,4,4-trimethylpentanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / LDA / tetrahydrofuran / 0.08 h / -78 °C

2: 100 percent / 23.5 h / 25 °C

With lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1016/S0040-4020(01)80401-4