Technology Process of (η5-1,2-diphenyl-4,5-dimethyl-1-hydrophosphorin 1-oxide)acetylcyclopentadienyliron
There total 1 articles about (η5-1,2-diphenyl-4,5-dimethyl-1-hydrophosphorin 1-oxide)acetylcyclopentadienyliron which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
acetyl chloride; AlCl3;
In
dichloromethane;
A mixt. of complex, AlCl3 and acetyl chloride was refluxed in CH2cl2 for 2 h, H2O was added (Ar atm.);; evapd., extd. from water layer with CH2Cl2, dried with MgSO4, evapd., chromd. on silica column with ether-methanol; elem. anal.;;