(η5-1,2-diphenyl-4,5-dimethyl-1-hydrophosphorin 1-oxide)cyclopentadienyliron

Base Information

Chemical Name:(η5-1,2-diphenyl-4,5-dimethyl-1-hydrophosphorin 1-oxide)cyclopentadienyliron
CAS No.:90245-12-8
Molecular Formula:C₂₄H₂₃FeOP
Molecular Weight:414.267
Hs Code.:

Synonyms:(η5-1,2-diphenyl-4,5-dimethyl-1-hydrophosphorin 1-oxide)cyclopentadienyliron

Suppliers and Price of (η5-1,2-diphenyl-4,5-dimethyl-1-hydrophosphorin 1-oxide)cyclopentadienyliron

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (η5-1,2-diphenyl-4,5-dimethyl-1-hydrophosphorin 1-oxide)cyclopentadienyliron

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (η5-1,2-diphenyl-4,5-dimethyl-1-hydrophosphorin 1-oxide)cyclopentadienyliron

There total 1 articles about (η5-1,2-diphenyl-4,5-dimethyl-1-hydrophosphorin 1-oxide)cyclopentadienyliron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 38117-54-3
cyclopentadienyl iron(II) dicarbonyl dimer

: 90219-11-7
1,2-diphenyl-4,5-dimethyl-1-hydrophosphorin oxide

: 90245-12-8
(η5-1,2-diphenyl-4,5-dimethyl-1-hydrophosphorin 1-oxide)cyclopentadienyliron

Guidance literature:: In xylene; A mixt. of reagents in xylene was refluxed for 20 h (Ar atm.), cooled;; filtered, evapd., chromd. on silica column with ether-ethyl acetate;;

Reference yield: 52.0%

: 90245-12-8
(η5-1,2-diphenyl-4,5-dimethyl-1-hydrophosphorin 1-oxide)cyclopentadienyliron

: 90245-10-6
(η5-1-butyl-2-phenyl-4,5-dimethyl-1-hydrophosphorin 1-oxide)cyclopentadienyliron

Guidance literature:: With n-butyllithium; HCl; In tetrahydrofuran; hexane; A soln. of complex in THF was treated at -70°C with n-BuLi in hexane, slowly warmed to 25°C; aq. HCl was added (Ar atm.);; evapd., extd. from water layer with CH2Cl2, dried with MgSO4, evapd., chromd. on silica column with ether-methanol; elem. anal.;;

Reference yield: 48.0%

: 90245-12-8
(η5-1,2-diphenyl-4,5-dimethyl-1-hydrophosphorin 1-oxide)cyclopentadienyliron

: 90245-11-7
(η5-1,2-diphenyl-4,5-dimethyl-1-hydrophosphorin 1-oxide)acetylcyclopentadienyliron

Guidance literature:: With acetyl chloride; AlCl₃; In dichloromethane; A mixt. of complex, AlCl3 and acetyl chloride was refluxed in CH2cl2 for 2 h, H2O was added (Ar atm.);; evapd., extd. from water layer with CH2Cl2, dried with MgSO4, evapd., chromd. on silica column with ether-methanol; elem. anal.;;