Benzyloxycarbonylamino-acetic acid 3,5-di-tert-butyl-4-hydroxy-phenyl ester

Base Information

Chemical Name:Benzyloxycarbonylamino-acetic acid 3,5-di-tert-butyl-4-hydroxy-phenyl ester
CAS No.:210840-41-8
Molecular Formula:C₂₄H₃₁NO₅
Molecular Weight:413.514
Hs Code.:

Synonyms:Benzyloxycarbonylamino-acetic acid 3,5-di-tert-butyl-4-hydroxy-phenyl ester

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Chemical Property of Benzyloxycarbonylamino-acetic acid 3,5-di-tert-butyl-4-hydroxy-phenyl ester

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Technology Process of Benzyloxycarbonylamino-acetic acid 3,5-di-tert-butyl-4-hydroxy-phenyl ester

There total 4 articles about Benzyloxycarbonylamino-acetic acid 3,5-di-tert-butyl-4-hydroxy-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: Benzyloxycarbonylamino-acetic acid 1,3,5-tri-tert-butyl-4-oxo-cyclohexa-2,5-dienyl ester

: Benzyloxycarbonylamino-acetic acid 3,5-di-tert-butyl-2-hydroxy-phenyl ester

: 210840-41-8
Benzyloxycarbonylamino-acetic acid 3,5-di-tert-butyl-4-hydroxy-phenyl ester

Guidance literature:: With Amberlyst 15; hydrogen cation; In toluene; at -20 - -10 ℃;
DOI:10.1016/S0040-4020(01)87054-X

Reference yield: 25.0%

: 2444-28-2
2,6-di-tert-butyl-4-hydroxyphenol

: 1138-80-3
N-(Benzyloxycarbonyl)glycine

: 210840-41-8
Benzyloxycarbonylamino-acetic acid 3,5-di-tert-butyl-4-hydroxy-phenyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; 1.) 0 deg C, 1 h, 2.) r.t., 24 h, 3.) 40 deg C, 72 h;
DOI:10.1515/znb-1998-0717

Reference yield:

: 732-26-3
2,4,6-tri-tert-butylphenoxol

: 210840-41-8
Benzyloxycarbonylamino-acetic acid 3,5-di-tert-butyl-4-hydroxy-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent Turnov_. / 2,6-lutidine, Et₄NBF₄ / CH₂Cl₂ / anodic oxidation (+1100 mV)

2: 65 percent / Amberlyst 15/H+ / toluene / -20 - -10 °C

With 2,6-dimethylpyridine; Amberlyst 15; hydrogen cation; N,N,N,N-tetraethylammonium tetrafluoroborate; In dichloromethane; toluene;
DOI:10.1016/S0040-4020(01)87054-X