1-methyl-3-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)-2,5,6-trichloroindole

Base Information

Chemical Name:1-methyl-3-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)-2,5,6-trichloroindole
CAS No.:917247-74-6
Molecular Formula:C₃₅H₃₂Cl₃NO₄
Molecular Weight:637.002
Hs Code.:

Synonyms:1-methyl-3-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)-2,5,6-trichloroindole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-methyl-3-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)-2,5,6-trichloroindole

Chemical Property:

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Technology Process of 1-methyl-3-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)-2,5,6-trichloroindole

There total 4 articles about 1-methyl-3-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)-2,5,6-trichloroindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 917247-73-5
3-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)-2,5,6-trichloroindole

: 74-88-4
methyl iodide

: 917247-74-6
1-methyl-3-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)-2,5,6-trichloroindole

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃; for 0.333333h;
DOI:10.1080/15257770500265646

Reference yield:

: 917247-69-9
1-acetyl-2,5,6-trichloroindole

: 917247-74-6
1-methyl-3-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)-2,5,6-trichloroindole

Guidance literature:: Multi-step reaction with 3 steps

1: 45 percent / BF₃*Et₂O / CH₂Cl₂ / 0.17 h / 0 °C

2: 99 percent / MeNH₂ / methanol / 0.5 h / 20 °C

3: 94 percent / NaH / tetrahydrofuran; various solvent(s) / 0.33 h / 0 - 20 °C

With boron trifluoride diethyl etherate; sodium hydride; methylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1080/15257770500265646

Reference yield:

: 917247-71-3
1-acetyl-3-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)-2,5,6-trichloroindole

: 917247-74-6
1-methyl-3-(2,3,5-tri-O-benzyl-β-D-ribofuranosyl)-2,5,6-trichloroindole

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / MeNH₂ / methanol / 0.5 h / 20 °C

2: 94 percent / NaH / tetrahydrofuran; various solvent(s) / 0.33 h / 0 - 20 °C

With sodium hydride; methylamine; In tetrahydrofuran; methanol;
DOI:10.1080/15257770500265646